6--6-methoxy-5-methyl-3-phenyl-6H-1,2-oxazine

Base Information

Chemical Name:6--6-methoxy-5-methyl-3-phenyl-6H-1,2-oxazine
CAS No.:133350-31-9
Molecular Formula:C₁₉H₁₉NO₃
Molecular Weight:309.365
Hs Code.:

6-<Hydroxy(phenyl)methyl>-6-methoxy-5-methyl-3-phenyl-6H-1,2-oxazine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 6--6-methoxy-5-methyl-3-phenyl-6H-1,2-oxazine

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Technology Process of 6--6-methoxy-5-methyl-3-phenyl-6H-1,2-oxazine

There total 4 articles about 6--6-methoxy-5-methyl-3-phenyl-6H-1,2-oxazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 56.0%

: 5,6-Dihydro-6--6-methoxy-5-methylene-3-phenyl-4H-1,2-oxazine

: 133350-31-9,133350-32-0
6--6-methoxy-5-methyl-3-phenyl-6H-1,2-oxazine

Guidance literature:: With triethylamine; In 1,4-dioxane; for 168h; Heating;

Reference yield:

: 21572-32-7
2-chloro-1-phenyl-ethanone oxime

: 133350-31-9,133350-32-0
6--6-methoxy-5-methyl-3-phenyl-6H-1,2-oxazine

Guidance literature:: Multi-step reaction with 2 steps

1: 28 percent / Na₂CO₃ / various solvent(s) / 192 h / Ambient temperature

2: 56 percent / Et₃N / dioxane / 168 h / Heating

With sodium carbonate; triethylamine; In 1,4-dioxane;

Reference yield:

: 100-52-7
benzaldehyde

: 133350-31-9,133350-32-0
6--6-methoxy-5-methyl-3-phenyl-6H-1,2-oxazine

Guidance literature:: Multi-step reaction with 3 steps

1: 1) n-BuLi

2: 28 percent / Na₂CO₃ / various solvent(s) / 192 h / Ambient temperature

3: 56 percent / Et₃N / dioxane / 168 h / Heating

With n-butyllithium; sodium carbonate; triethylamine; In 1,4-dioxane;