aci-nitroethane trimethylsilyl ester

Base Information

• Chemical Name: aci-nitroethane trimethylsilyl ester
• CAS No.: 51146-36-2
• Molecular Formula: C₅H₁₃NO₂Si
• Molecular Weight: 147.249
• Mol file: 51146-36-2.mol

Synonyms:

Chemical Property of aci-nitroethane trimethylsilyl ester

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of aci-nitroethane trimethylsilyl ester

There total 6 articles about aci-nitroethane trimethylsilyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

Tetraethyl methylenediphosphonate (1660-94-2) + 1-chloro-4-(2-nitropropenyl)benzene (710-20-3) → tetraethyl<(p-chlorophenyl)vinylidene>bisphosphonate (53235-89-5) + aci-nitroethane trimethylsilyl ester (51146-36-2,65275-13-0,65275-14-1)

Guidance literature:

Yield given. Multistep reaction;

Reference yield:

Tetraethyl methylenediphosphonate (1660-94-2) + 1-(p-nitrophenyl)-2-nitro-1-propene (4231-16-7) → tetraethyl 2-(4-nitrophenyl)ethene-1,1-diyldiphosphonate (53359-85-6) + aci-nitroethane trimethylsilyl ester (51146-36-2,65275-13-0,65275-14-1)

Guidance literature:

Yield given. Multistep reaction;

Reference yield:

Tetraethyl methylenediphosphonate (1660-94-2) + 2-nitro-1-(4'-dimethylaminophenyl)-1-propene (52287-57-7,29440-69-5) → aci-nitroethane trimethylsilyl ester (51146-36-2,65275-13-0,65275-14-1) + [1-(Diethoxy-phosphoryl)-2-(4-dimethylamino-phenyl)-vinyl]-phosphonic acid diethyl ester (95601-02-8)

Guidance literature:

Yield given. Multistep reaction;

upstream raw materials:

Tetraethyl methylenediphosphonate

(2-nitroprop-1-enyl)benzene

4-(2-nitro-propenyl)-anisole

1-chloro-4-(2-nitropropenyl)benzene

Downstream raw materials:

1-Phenyl-2-nitropropyl-trimethylsilylaether