O²,O³,O⁵-trimethyl-D-gluconic acid-(N'-phenyl-hydrazide)

Base Information

• Chemical Name: O²,O³,O⁵-trimethyl-D-gluconic acid-(N'-phenyl-hydrazide)
• CAS No.: 131516-91-1
• Molecular Formula: C₁₅H₂₄N₂O₆
• Molecular Weight: 328.365
• Mol file: 131516-91-1.mol

Synonyms:

Chemical Property of O²,O³,O⁵-trimethyl-D-gluconic acid-(N'-phenyl-hydrazide)

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of O²,O³,O⁵-trimethyl-D-gluconic acid-(N'-phenyl-hydrazide)

There total 4 articles about O²,O³,O⁵-trimethyl-D-gluconic acid-(N'-phenyl-hydrazide) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

phenylhydrazine (100-63-0) + O2,O3,O5-trimethyl-D-gluconic acid-4-lactone (898283-34-6) → O2,O3,O5-trimethyl-D-gluconic acid-(N'-phenyl-hydrazide) (131516-91-1)

Guidance literature:

DOI:10.1039/jr9440000571 DOI:10.1021/ja01211a085

Reference yield:

O2,O3,O5-Trimethyl-D-glucose (51885-67-7) → O2,O3,O5-trimethyl-D-gluconic acid-(N'-phenyl-hydrazide) (131516-91-1)

Guidance literature:

Multi-step reaction with 2 steps

1: water; bromine; lead (II)-carbonate / Erhitzen des Reaktionsprodukts

With lead(II) carbonate; water; bromine;

DOI:10.1039/jr9440000571

Reference yield:

O2,O3,O5-Trimethyl-D-galactose (34897-30-8) → O2,O3,O5-trimethyl-D-galactonic acid-(N'-phenyl-hydrazide) (131516-91-1)

Guidance literature:

Multi-step reaction with 2 steps

1: water; bromine / Erhitzen des Reaktionsprodukts unter 0.01 Torr auf 170grad

With water; bromine;

DOI:10.1039/jr9400001114

upstream raw materials:

phenylhydrazine

O²,O³,O⁵-trimethyl-D-gluconic acid-4-lactone

O²,O³,O⁵-Trimethyl-D-glucose

O²,O³,O⁵-trimethyl-D-galactonic acid-4-lactone