Phosphoric acid dibenzyl ester (1R,2R,4S,5S,6R)-2,5-bis-benzyloxy-6-(bis-benzyloxy-phosphoryloxy)-3-oxo-4-triethylsilanyloxy-cyclohexyl ester

Base Information

Chemical Name:Phosphoric acid dibenzyl ester (1R,2R,4S,5S,6R)-2,5-bis-benzyloxy-6-(bis-benzyloxy-phosphoryloxy)-3-oxo-4-triethylsilanyloxy-cyclohexyl ester
CAS No.:120065-89-6
Molecular Formula:C₅₄H₆₂O₁₂P₂Si
Molecular Weight:993.112
Hs Code.:

Phosphoric acid dibenzyl ester (1R,2R,4S,5S,6R)-2,5-bis-benzyloxy-6-(bis-benzyloxy-phosphoryloxy)-3-oxo-4-triethylsilanyloxy-cyclohexyl ester

Synonyms:

Suppliers and Price of Phosphoric acid dibenzyl ester (1R,2R,4S,5S,6R)-2,5-bis-benzyloxy-6-(bis-benzyloxy-phosphoryloxy)-3-oxo-4-triethylsilanyloxy-cyclohexyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of Phosphoric acid dibenzyl ester (1R,2R,4S,5S,6R)-2,5-bis-benzyloxy-6-(bis-benzyloxy-phosphoryloxy)-3-oxo-4-triethylsilanyloxy-cyclohexyl ester

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of Phosphoric acid dibenzyl ester (1R,2R,4S,5S,6R)-2,5-bis-benzyloxy-6-(bis-benzyloxy-phosphoryloxy)-3-oxo-4-triethylsilanyloxy-cyclohexyl ester

There total 10 articles about Phosphoric acid dibenzyl ester (1R,2R,4S,5S,6R)-2,5-bis-benzyloxy-6-(bis-benzyloxy-phosphoryloxy)-3-oxo-4-triethylsilanyloxy-cyclohexyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 141725-53-3
Phosphoric acid dibenzyl ester (1R,2S,3R,4R,5S,6R)-2,5-bis-benzyloxy-6-(bis-benzyloxy-phosphoryloxy)-3-hydroxy-4-triethylsilanyloxy-cyclohexyl ester

: 120065-89-6,128051-59-2
Phosphoric acid dibenzyl ester (1R,2R,4S,5S,6R)-2,5-bis-benzyloxy-6-(bis-benzyloxy-phosphoryloxy)-3-oxo-4-triethylsilanyloxy-cyclohexyl ester

Guidance literature:: With acetic anhydride; dimethyl sulfoxide; In benzene; Heating;
DOI:10.1016/S0040-4039(00)80731-5

Reference yield:

: 990-91-0
dibenzyl [[bis(benzyloxy)phosphoryl]oxy]phosphonate

: 120065-89-6,128051-59-2
Phosphoric acid dibenzyl ester (1R,2R,4S,5S,6R)-2,5-bis-benzyloxy-6-(bis-benzyloxy-phosphoryloxy)-3-oxo-4-triethylsilanyloxy-cyclohexyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: 81 percent / n-BuLi

2: CF₃COOH / methanol / Ambient temperature

3: 95 percent / pyridine

4: 86 percent / DMSO, acetic anhydride / benzene / Heating

With pyridine; n-butyllithium; acetic anhydride; dimethyl sulfoxide; trifluoroacetic acid; In methanol; benzene;
DOI:10.1016/S0040-4039(00)80731-5

Reference yield:

: 994-30-9
triethylsilyl chloride

: 120065-89-6,128051-59-2
Phosphoric acid dibenzyl ester (1R,2R,4S,5S,6R)-2,5-bis-benzyloxy-6-(bis-benzyloxy-phosphoryloxy)-3-oxo-4-triethylsilanyloxy-cyclohexyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 95 percent / pyridine

2: 86 percent / DMSO, acetic anhydride / benzene / Heating

With pyridine; acetic anhydride; dimethyl sulfoxide; In benzene;
DOI:10.1016/S0040-4039(00)80731-5