2,5-Bis-4-(1-methyl-2-oxo-4-carboethoxybutyl)toluene

Base Information

• Chemical Name: 2,5-Bis-4-(1-methyl-2-oxo-4-carboethoxybutyl)toluene
• CAS No.: 88589-41-7
• Molecular Formula: C₄₃H₄₆N₂O₇S₂
• Molecular Weight: 766.979

Synonyms:

Chemical Property of 2,5-Bis-4-(1-methyl-2-oxo-4-carboethoxybutyl)toluene

Chemical Property:

Purity/Quality:

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Technology Process of 2,5-Bis-4-(1-methyl-2-oxo-4-carboethoxybutyl)toluene

There total 3 articles about 2,5-Bis-4-(1-methyl-2-oxo-4-carboethoxybutyl)toluene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 5.0%

ethanol (64-17-5) + 2,5-Bis-4-(2,5-dioxo-1-methylcyclopentyl)toluene (88589-36-0) → 4-Benzyl-7--6,8b-dimethyl-3a-hydroxy-1-oxo-1,2,3,3a,4,8b-hexahydrocyclopentindole (88589-37-1) + 2,5-Bis-4-(1-methyl-2-oxo-4-carboethoxybutyl)toluene (88589-41-7)

Guidance literature:

With tetraethylammonium tosylate; In N,N-dimethyl-formamide; for 0.116667h; electrolysis with Pb cathode at -1.7 V vs. Pt;

DOI:10.1021/jo00180a001

Reference yield:

C27H28N2O6S2 (72374-10-8) → 2,5-Bis-4-(1-methyl-2-oxo-4-carboethoxybutyl)toluene (88589-41-7)

Guidance literature:

Multi-step reaction with 2 steps

1: 98 percent / K₂CO₃, KI / acetone / 72 h / Heating

2: 63 percent / 0.04 M Et₄NOTs / dimethylformamide / 0.12 h / electrolysis with Pb cathode at -1.7 V vs. Pt

With potassium carbonate; tetraethylammonium tosylate; potassium iodide; In N,N-dimethyl-formamide; acetone;

DOI:10.1021/jo00180a001

Reference yield:

benzyl bromide (100-39-0) → 2,5-Bis-4-(1-methyl-2-oxo-4-carboethoxybutyl)toluene (88589-41-7)

Guidance literature:

Multi-step reaction with 2 steps

1: 98 percent / K₂CO₃, KI / acetone / 72 h / Heating

2: 63 percent / 0.04 M Et₄NOTs / dimethylformamide / 0.12 h / electrolysis with Pb cathode at -1.7 V vs. Pt

With potassium carbonate; tetraethylammonium tosylate; potassium iodide; In N,N-dimethyl-formamide; acetone;

DOI:10.1021/jo00180a001

upstream raw materials:

ethanol

2,5-Bis-4-(2,5-dioxo-1-methylcyclopentyl)toluene

C₂₇H₂₈N₂O₆S₂

benzyl bromide

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