N'-((6-bromoimidazo[1,2-a]pyridin-3-yl)methylene)-N,2-dimethyl-5-nitrobenzenesulfonohydrazide

Base Information

Chemical Name:N'-((6-bromoimidazo[1,2-a]pyridin-3-yl)methylene)-N,2-dimethyl-5-nitrobenzenesulfonohydrazide
CAS No.:1201670-42-9
Molecular Formula:C₁₆H₁₄BrN₅O₄S
Molecular Weight:452.288
Hs Code.:
UNII:NT63XAU01R
Nikkaji Number:J2.482.103J
Pharos Ligand ID:AGUT8SFL54ZF

Synonyms:PIK 75;PIK-75

Suppliers and Price of N'-((6-bromoimidazo[1,2-a]pyridin-3-yl)methylene)-N,2-dimethyl-5-nitrobenzenesulfonohydrazide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of N'-((6-bromoimidazo[1,2-a]pyridin-3-yl)methylene)-N,2-dimethyl-5-nitrobenzenesulfonohydrazide

Chemical Property:

XLogP3:3.8
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:7
Rotatable Bond Count:4
Exact Mass:450.99499
Heavy Atom Count:27
Complexity:679

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CC1=C(C=C(C=C1)[N+](=O)[O-])S(=O)(=O)N(C)N=CC2=CN=C3N2C=C(C=C3)Br
Isomeric SMILES:CC1=C(C=C(C=C1)[N+](=O)[O-])S(=O)(=O)N(C)/N=C\C2=CN=C3N2C=C(C=C3)Br

Technology Process of N'-((6-bromoimidazo[1,2-a]pyridin-3-yl)methylene)-N,2-dimethyl-5-nitrobenzenesulfonohydrazide

There total 3 articles about N'-((6-bromoimidazo[1,2-a]pyridin-3-yl)methylene)-N,2-dimethyl-5-nitrobenzenesulfonohydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 186581-53-3,908094-01-9,334-88-3
diazomethane

: 945619-40-9
N'-((6-bromoimidazo[1,2-a]pyridin-3-yl)methylene)-2-methyl-5-nitrobenzenesulfonohydrazide

: 1201670-42-9,945619-31-8
PIK-75

Guidance literature:: In tetrahydrofuran; diethyl ether;
DOI:10.1016/j.bmc.2007.08.062

Reference yield: 43.0%

: 945619-40-9
N'-((6-bromoimidazo[1,2-a]pyridin-3-yl)methylene)-2-methyl-5-nitrobenzenesulfonohydrazide

: 74-88-4
methyl iodide

: 1201670-42-9,945619-31-8
PIK-75

Guidance literature:: With sodium hydride; In N,N-dimethyl-formamide; for 0.166667h;
DOI:10.1016/j.bmc.2007.05.070

Reference yield: 10.0%

: 30384-96-4
6-bromoimidazo[1,2-a]pyridine-3-carbaldehyde

: 121-02-8
2-methyl-5-nitrobenzene-1-sulfonyl chloride

: 60-34-4
methylhydrazine

: 372196-67-3,1201670-42-9,945619-31-8
[2-methyl-5-nitro-1-benzenesulfonic acid 2-[(6-bromoimidazo[1,2-a]pyridin-3-yl)methylene]-1-methylhydrazide]

Guidance literature:: 6-bromoimidazo[1,2-a]pyridine-3-carbaldehyde; methylhydrazine; In ethanol; for 3h; Reflux;

2-methyl-5-nitrobenzene-1-sulfonyl chloride; With pyridine; at 20 ℃; for 4h;
DOI:10.1002/anie.201804917