Technology Process of C15H10Li2
There total 6 articles about C15H10Li2 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 6 steps
1: 77 percent / triphenylphosphine / benzene / 50 h / 140 °C
2: 78 percent / tri-n-butyltin hydride / pentane / 24 h / 25 °C
3: 19 percent / 50percent aq. NaOH, cetrimide / 48 h / 5 - 25 °C
4: 70 percent / n-butyllithium / tetrahydrofuran / -100 °C
5: n-butyllithium / tetrahydrofuran / -100 °C
6: t-butyllithium / tetrahydrofuran / -30 °C
With
sodium hydroxide; n-butyllithium; tert.-butyl lithium; tri-n-butyl-tin hydride; cetyltrimethylammonim bromide; triphenylphosphine;
In
tetrahydrofuran; pentane; benzene;
DOI:10.1016/0040-4039(95)01852-9
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 19 percent / 50percent aq. NaOH, cetrimide / 48 h / 5 - 25 °C
2: 70 percent / n-butyllithium / tetrahydrofuran / -100 °C
3: n-butyllithium / tetrahydrofuran / -100 °C
4: t-butyllithium / tetrahydrofuran / -30 °C
With
sodium hydroxide; n-butyllithium; tert.-butyl lithium; cetyltrimethylammonim bromide;
In
tetrahydrofuran;
DOI:10.1016/0040-4039(95)01852-9