N--L-alanyl>-N'-<(tert-butyloxy)carbonyl>hexane-1,6-diamine

Base Information

Chemical Name:N--L-alanyl>-N'-<(tert-butyloxy)carbonyl>hexane-1,6-diamine
CAS No.:145118-12-3
Molecular Formula:C₂₂H₃₅N₃O₅
Molecular Weight:421.537
Hs Code.:

N-<N-<(Benzyloxy)carbonyl>-L-alanyl>-N'-<(tert-butyloxy)carbonyl>hexane-1,6-diamine

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Chemical Property of N--L-alanyl>-N'-<(tert-butyloxy)carbonyl>hexane-1,6-diamine

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Technology Process of N--L-alanyl>-N'-<(tert-butyloxy)carbonyl>hexane-1,6-diamine

There total 2 articles about N--L-alanyl>-N'-<(tert-butyloxy)carbonyl>hexane-1,6-diamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1142-20-7
N-Cbz-Ala

: 145118-12-3
N--L-alanyl>-N'-<(tert-butyloxy)carbonyl>hexane-1,6-diamine

Guidance literature:: Multi-step reaction with 2 steps

1: Et₃N / tetrahydrofuran / 0.17 h / -20 - -15 °C

2: Et₃N / tetrahydrofuran; H₂O / 18 h / Ambient temperature

With triethylamine; In tetrahydrofuran; water;
DOI:10.1002/hlca.19920750617

Reference yield:

: 65638-93-9
N-Carbobenzoxy-L-alanin-kohlensaeureaethylesteranhydrid

: 65915-94-8
N-(tert-butoxycarbonyl)-1,6-diaminohexane hydrochloride

: 145118-12-3
N--L-alanyl>-N'-<(tert-butyloxy)carbonyl>hexane-1,6-diamine

Guidance literature:: With triethylamine; In tetrahydrofuran; water; for 18h; Yield given; Ambient temperature;
DOI:10.1002/hlca.19920750617

Reference yield:

: 145118-12-3
N--L-alanyl>-N'-<(tert-butyloxy)carbonyl>hexane-1,6-diamine

: Iaa(5-BnO)->Ala->Dhx

Guidance literature:: Multi-step reaction with 3 steps

1: 98.6 percent / H₂ / 10percent Pd/C / methanol / 20 h

2: Et₃N / tetrahydrofuran / 18 h / Ambient temperature

3: HCl / dioxane / 0.67 h

With hydrogenchloride; hydrogen; triethylamine; palladium on activated charcoal; In tetrahydrofuran; 1,4-dioxane; methanol;
DOI:10.1002/hlca.19920750617