6-Ph-nido-5,6,9-C₃B₇H₁₀

Base Information

Chemical Name:6-Ph-nido-5,6,9-C₃B₇H₁₀
CAS No.:173166-46-6
Molecular Formula:C₉H₁₅B₇
Molecular Weight:198.895
Hs Code.:

6-Ph-nido-5,6,9-C<sub>3</sub>B<sub>7</sub>H<sub>10</sub>

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Chemical Property of 6-Ph-nido-5,6,9-C₃B₇H₁₀

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Technology Process of 6-Ph-nido-5,6,9-C₃B₇H₁₀

There total 1 articles about 6-Ph-nido-5,6,9-C₃B₇H₁₀ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 37.0%

: 7647-01-0,15364-23-5
hydrogenchloride

: 17653-38-2
C₂B₇H₁₃

: lithium hydride

: 100-47-0
benzonitrile

: 173166-46-6
6-Ph-nido-5,6,9-C₃B₇H₁₀

Guidance literature:: In 1,2-dimethoxyethane; under N2 atm. arachno-4,6-C2B7H13 and LiH in glyme was stirred at room temp. for 45 min, filtered, PhCN was added and heated at reflux for 2 days, solvent was evapd., residue was dissolved in CH2Cl2, 1 M HCl in Et2O was added, 20 min at 0°C; solvent was evapd.;
DOI:10.1021/ic049827a