triphenylphosphine-dicarbonyl(1-2-η:3-4-η-1,4-diphenyl-1-azabuta-1,3-diene)iron

Base Information

Chemical Name:triphenylphosphine-dicarbonyl(1-2-η:3-4-η-1,4-diphenyl-1-azabuta-1,3-diene)iron
CAS No.:12119-27-6
Molecular Formula:C₃₅H₂₈FeNO₂P
Molecular Weight:581.434
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of triphenylphosphine-dicarbonyl(1-2-η:3-4-η-1,4-diphenyl-1-azabuta-1,3-diene)iron

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Technology Process of triphenylphosphine-dicarbonyl(1-2-η:3-4-η-1,4-diphenyl-1-azabuta-1,3-diene)iron

There total 4 articles about triphenylphosphine-dicarbonyl(1-2-η:3-4-η-1,4-diphenyl-1-azabuta-1,3-diene)iron which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: (C₆H₅)CHCHCHN(C₆H₅)*Fe(CO)3=(C₆H₅)CHCHCHN(C₆H₅)Fe(CO)3

: 14741-34-5,21255-52-7
tricarbonyl bis(triphenylphosphine) iron

: 315181-26-1,12119-27-6
(C₆H₅)CHCHCHN(C₆H₅)*Fe(CO)2(P(C₆H₅)3)=(C₆H₅)CHCHCHN(C₆H₅)Fe(CO)2(P(C₆H₅)3)

Guidance literature:: With triphenylphosphine; In benzene; at 60 - 80 °C,with excess of P(C6H5)3; recrystn. from non-polar solvent or sepn. by chromy. on Al2O3, eluent CH2Cl2/C6H14;

Reference yield:

: 12112-97-9
tricarbonyl[(1-4-η)-1,4-diphenyl-1-azabuta-1,3-diene]iron

: 14741-34-5,21255-52-7
tricarbonyl bis(triphenylphosphine) iron

: 12119-27-6,315181-26-1
triphenylphosphine-dicarbonyl(1-2-η:3-4-η-1,4-diphenyl-1-azabuta-1,3-diene)iron

Guidance literature:: With triphenylphosphine; In toluene; byproducts: CO, PhCH=CH-CH=NPh; deaerated solvent, excess PPh3, 49.5-70.2°C; not isolated, reaction followed by IR spectroscopy; Kinetics;
DOI:10.1039/DT9770002181