trans-Mo2(μ-N,N′-bis(4-methoxyphenyl)formamidinato-κ2N:N′)2(OOCCH3)2

Base Information

Chemical Name:trans-Mo2(μ-N,N′-bis(4-methoxyphenyl)formamidinato-κ2N:N′)2(OOCCH3)2
CAS No.:679398-07-3
Molecular Formula:C₃₄H₃₆Mo₂N₄O₈
Molecular Weight:820.562
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of trans-Mo2(μ-N,N′-bis(4-methoxyphenyl)formamidinato-κ2N:N′)2(OOCCH3)2

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Technology Process of trans-Mo2(μ-N,N′-bis(4-methoxyphenyl)formamidinato-κ2N:N′)2(OOCCH3)2

There total 5 articles about trans-Mo2(μ-N,N′-bis(4-methoxyphenyl)formamidinato-κ2N:N′)2(OOCCH3)2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 14221-06-8,744215-74-5
tetrakis(acetato)dimolybdenum(II)

: 1152-75-6,141417-87-0
N,N'-bis(4-methoxyphenyl)iminoformamide

: 679404-52-5,679398-07-3
trans-[Mo₂(N,N'-di(p-anisyl)formamidinate)2(O₂CCH₃)2]

Guidance literature:: With NaOCH₃; In tetrahydrofuran; methanol; under N2atm. to suspn. Mo2(OAc)4 and N,N'-di-p-anisylformamidine in THF soln. NaOMe in MeOH was added and stirred for 5 h at room temp.; solvent was removed in vacuo, CH2Cl2 was added, soln. was filtered andconcd., EtOH was added, ppt. was washed with EtOH and hexane, and dried invacuo; elem. anal.;
DOI:10.1021/ic035433s

Reference yield: 83.0%

: [cis-Mo₂(N,N'-di-p-anisylformamidinato)2(acetonitrile)4](BF₄)2

: 127-09-3
sodium acetate

: 679398-07-3,679404-52-5
cis-Mo₂(N,N'-di-p-anisylformamidinate)2(O₂CCH₃)2

Guidance literature:: In acetonitrile; under N2 atm. to cis-(Mo2(DAniF)2(MeCN)4)(BF4)2 AcONa in MeCN was added and stirred at room for 2 h; ppt. was filtered, extd. with CH2Cl2, hexane was added, ppt. was filtered and dried in vacuo; elem. anal.;
DOI:10.1021/ic035433s

Reference yield:

: 14221-06-8,744215-74-5
tetrakis(acetato)dimolybdenum(II)

: 1152-75-6,141417-87-0
N,N'-bis(4-methoxyphenyl)iminoformamide

: 679404-52-5,679398-07-3
trans-Mo2(μ-N,N′-bis(4-methoxyphenyl)formamidinato-κ2N:N′)2(OOCCH3)2

Guidance literature:: With sodium methylate; In tetrahydrofuran; methanol; for 2h; Inert atmosphere; Schlenk technique;
DOI:10.1007/s10870-017-0698-7