Re₂(N,N'-di(3-methoxyphenyl)formamidine^(1-))2Cl₄

Base Information

• Chemical Name: Re₂(N,N'-di(3-methoxyphenyl)formamidine^(1-))2Cl₄
• CAS No.: 913355-99-4
• Molecular Formula: C₃₀H₃₀Cl₄N₄O₄Re₂
• Molecular Weight: 1024.82

Synonyms:

Chemical Property of Re₂(N,N'-di(3-methoxyphenyl)formamidine^(1-))2Cl₄

Chemical Property:

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Technology Process of Re₂(N,N'-di(3-methoxyphenyl)formamidine^(1-))2Cl₄

There total 1 articles about Re₂(N,N'-di(3-methoxyphenyl)formamidine^(1-))2Cl₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

tetra-n-butylammonium octachlorodirhenate(III) (14023-10-0) + N,N'-di-(3-methoxy)phenylformamidine → Re2(N,N'-di(3-methoxyphenyl)formamidine(1-))2Cl4 (913355-99-4)

Guidance literature:

In neat (no solvent); (under Ar); Re-complex and ligand heated at 150°C for 36 h; ppt. extd. with CH2Cl2, dissolved in THF, recrystd. from hexane/THF, filtrate rotovapped, ppt. washed with hot EtOH, recrystd. from Et2O/THF; elem. anal.;

DOI:10.1016/j.ica.2006.06.044

upstream raw materials:

tetra-n-butylammonium octachlorodirhenate(III)

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