3,3,3-trifluoropropyl methansulfonate

Base Information

• Chemical Name: 3,3,3-trifluoropropyl methansulfonate
• CAS No.: 911116-16-0
• Molecular Formula: C4H7F3O3S
• Molecular Weight: 192.159
• Hs Code.: 2905590090
• Mol file: 911116-16-0.mol

Synonyms:3,3,3-trifluoropropyl methansulfonate;Methanesulfonic acid 3,3,3-trifluoro-propyl ester;

Chemical Property of 3,3,3-trifluoropropyl methansulfonate

Chemical Property:

• Vapor Pressure: 0.241mmHg at 25°C
• Boiling Point: 213.3oC at 760 mmHg
• Flash Point: 82.8oC
• PSA: 51.75000
• Density: 1.388g/cm3
• LogP: 1.99580

Purity/Quality:

98%Min ^*data from raw suppliers

3,3,3-TrifluoropropylMethanesulfonate ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 3,3,3-trifluoropropyl methansulfonate

There total 2 articles about 3,3,3-trifluoropropyl methansulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

3,3,3-Trifluoropropanol (2240-88-2) + methanesulfonyl chloride (124-63-0) → 3,3,3-trifluoropropyl methanesulfonate (911116-16-0)

Guidance literature:

With triethylamine; In dichloromethane; at 0 - 20 ℃; for 3h;

Reference yield:

→ 3,3,3-trifluoropropyl methanesulfonate (911116-16-0)

Guidance literature:

Reference yield: 84.6%

3,3,3-trifluoropropyl methanesulfonate (911116-16-0) + 3-methyl-8-(3-(trifluoromethoxy)phenoxy)-7-((2-(trimethylsilyl)ethoxy)methyl)-1H-purine-2,6(3H,7H)-dione → 3-methyl-8-(3-(trifluoromethoxy)phenoxy)-1-(3,3,3-trifluoropropyl)-7-((2-(trimethylsilyl)ethoxy)methyl)-1H-purine-2,6(3H,7H)-dione

Guidance literature:

With potassium carbonate; In N,N-dimethyl-formamide; at 60 ℃;

upstream raw materials:

3,3,3-Trifluoropropanol

methanesulfonyl chloride

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