Technology Process of C25H29F2N7O2
There total 5 articles about C25H29F2N7O2 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
p-Methoxybenzyl bromide;
With
sodium azide;
In
dimethyl sulfoxide;
at 20 ℃;
for 6h;
1-(1H-1,2,4-triazole-1-yl)-2-(2,4-difluorophenyl)-3-(N-propyl-N-propargylamino)-2-propanol;
With
copper(ll) sulfate pentahydrate; sodium L-ascorbate;
In
water; dimethyl sulfoxide;
at 20 ℃;
for 2h;
DOI:10.1039/c3ra41310a
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: sodium hydroxide; cetyltrimethylammonim bromide / toluene / 3 h / 60 °C
1.2: 1 h / 0 °C
2.1: triethylamine / ethanol / 6 h / Reflux
3.1: potassium iodide; potassium carbonate / acetonitrile / 6 h / 20 °C
4.1: sodium azide / dimethyl sulfoxide / 6 h / 20 °C
4.2: 2 h / 20 °C
With
sodium azide; cetyltrimethylammonim bromide; potassium carbonate; triethylamine; potassium iodide; sodium hydroxide;
In
ethanol; dimethyl sulfoxide; toluene; acetonitrile;
DOI:10.1039/c3ra41310a
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: triethylamine / ethanol / 6 h / Reflux
2.1: potassium iodide; potassium carbonate / acetonitrile / 6 h / 20 °C
3.1: sodium azide / dimethyl sulfoxide / 6 h / 20 °C
3.2: 2 h / 20 °C
With
sodium azide; potassium carbonate; triethylamine; potassium iodide;
In
ethanol; dimethyl sulfoxide; acetonitrile;
DOI:10.1039/c3ra41310a
