2-(dimesitylboryl)benzylidenemonoethanolamine

Base Information

• Chemical Name: 2-(dimesitylboryl)benzylidenemonoethanolamine
• CAS No.: 1232575-44-8
• Molecular Formula: C₂₇H₃₂BNO
• Molecular Weight: 397.368
• Mol file: 1232575-44-8.mol

Synonyms:

Chemical Property of 2-(dimesitylboryl)benzylidenemonoethanolamine

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2-(dimesitylboryl)benzylidenemonoethanolamine

There total 4 articles about 2-(dimesitylboryl)benzylidenemonoethanolamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

2-(dimesitylborane)benzaldehyde (1232575-38-0) + ethanolamine (141-43-5) → 2-(dimesitylboryl)benzylidenemonoethanolamine (1232575-44-8)

Guidance literature:

In toluene; HOCH2CH2NH2 added to a toluene soln. of 2-(dimesitylboryl)benzaldehyde at room temp.; stirred for 3 h; evapn. do dryness; recrystd. from CHCl3; elem. anal.;

DOI:10.1515/znb-2009-11-1219

Reference yield:

2-(2-bromophenyl)-1,3-dioxolan (34824-58-3) → 2-(dimesitylboryl)benzylidenemonoethanolamine (1232575-44-8)

Guidance literature:

Multi-step reaction with 3 steps

1: n-BuLi / hexane; diethyl ether

2: HCl / water; tetrahydrofuran

3: toluene

With n-BuLi; HCl; In tetrahydrofuran; diethyl ether; hexane; water; toluene;

DOI:10.1515/znb-2009-11-1219

Reference yield:

2-(2-dimesitylborylphenyl)-1,3-dioxolane (1232575-35-7) → 2-(dimesitylboryl)benzylidenemonoethanolamine (1232575-44-8)

Guidance literature:

Multi-step reaction with 2 steps

1: HCl / water; tetrahydrofuran

2: toluene

With HCl; In tetrahydrofuran; water; toluene;

DOI:10.1515/znb-2009-11-1219

upstream raw materials:

2-(dimesitylborane)benzaldehyde

ethanolamine

2-(2-bromophenyl)-1,3-dioxolan

2-(2-dimesitylborylphenyl)-1,3-dioxolane