Technology Process of C22H37NO2
There total 3 articles about C22H37NO2 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: potassium carbonate; 18-crown-6 ether / acetone / 12 h / 70 °C / Reflux
2.1: pyridinium chlorochromate / dichloromethane / 1 h / 20 °C
3.1: potassium tert-butylate / tetrahydrofuran / 0.33 h / Inert atmosphere
3.2: 0.5 h / 20 °C / Inert atmosphere
4.1: tetrahydrofuran / 24 h / 20 °C
With
18-crown-6 ether; potassium tert-butylate; potassium carbonate; pyridinium chlorochromate;
In
tetrahydrofuran; dichloromethane; acetone;
DOI:10.1021/ja404940s
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: pyridinium chlorochromate / dichloromethane / 1 h / 20 °C
2.1: potassium tert-butylate / tetrahydrofuran / 0.33 h / Inert atmosphere
2.2: 0.5 h / 20 °C / Inert atmosphere
3.1: tetrahydrofuran / 24 h / 20 °C
With
potassium tert-butylate; pyridinium chlorochromate;
In
tetrahydrofuran; dichloromethane;
DOI:10.1021/ja404940s