(4S,5S,R/S)-(+)-(2'-furyl)acetonitrile

Base Information

Chemical Name:(4S,5S,R/S)-(+)-(2'-furyl)acetonitrile
CAS No.:124686-45-9
Molecular Formula:C₁₉H₂₂N₂O₃
Molecular Weight:326.395
Hs Code.:

(4S,5S,R/S)-(+)-<N-(2,2-dimethyl-4-phenyl-1,2-dioxan-5-yl)-N-methylamino>(2'-furyl)acetonitrile

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (4S,5S,R/S)-(+)-(2'-furyl)acetonitrile

Chemical Property:

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Technology Process of (4S,5S,R/S)-(+)-(2'-furyl)acetonitrile

There total 2 articles about (4S,5S,R/S)-(+)-(2'-furyl)acetonitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 98-01-1
furfural

: 124686-47-1
(4S,5S)-(+)-2,2-Dimethyl-5-methylamino-4-phenyl-1,3-dioxan

: 151-50-8
potassium cyanide

: 124686-45-9,144951-59-7
(4S,5S,R/S)-(+)-(2'-furyl)acetonitrile

Guidance literature:: With hydrogenchloride; In methanol; water; pH 5-7, 0 deg C, then room t.;
DOI:10.1055/s-1995-3968

Reference yield:

: 98-01-1
furfural

: 151-50-8
potassium cyanide

: ((4S,5S)-2,2-Dimethyl-4-phenyl-[1,3]dioxan-5-yl)-methyl-amine; hydrochloride

: 124686-45-9,144951-59-7
(4S,5S,R/S)-(+)-(2'-furyl)acetonitrile

Guidance literature:: In water; 0 deg C -> room temp.;

Reference yield:

: 930-68-7
cyclohexenone

: 124686-45-9,144951-59-7
(4S,5S,R/S)-(+)-(2'-furyl)acetonitrile

: 100-39-0
benzyl bromide

: (S)-((1R,2S)-2-Benzyl-3-oxo-cyclohexyl)-[((4S,5S)-2,2-dimethyl-4-phenyl-[1,3]dioxan-5-yl)-methyl-amino]-furan-2-yl-acetonitrile

Guidance literature:: With lithium diisopropyl amide; Yield given. Multistep reaction; 1.) THF, -78 deg C, 1 h, 2.) THF, -78 deg C, 2 h, 3.) THF, HMPA, 30 min, -78 deg C to 0 deg C;
DOI:10.1055/s-1995-3968