1,2-dihydrofullerene functionalized with ethylester acetate group

Base Information

Chemical Name:1,2-dihydrofullerene functionalized with ethylester acetate group
CAS No.:161432-01-5
Molecular Formula:C₆₄H₈O₂
Molecular Weight:808.766
Hs Code.:

Synonyms:

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Chemical Property of 1,2-dihydrofullerene functionalized with ethylester acetate group

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Technology Process of 1,2-dihydrofullerene functionalized with ethylester acetate group

There total 1 articles about 1,2-dihydrofullerene functionalized with ethylester acetate group which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 17.2%

: 105-36-2
ethyl bromoacetate

: 99685-96-8,161105-99-3,161106-00-9,111138-12-6,133318-63-5,134053-11-5,134931-35-4,134931-36-5,139703-76-7,145633-27-8,175414-73-0,175414-74-1,175414-75-2,175519-12-7,175519-13-8,175519-14-9,175519-15-0,136376-46-0,144906-37-6,144906-38-7,151767-00-9,152882-97-8,152882-98-9,152882-99-0,153062-34-1,154171-74-1,154171-75-2,154333-99-0,154334-00-6,154397-63-4,154460-59-0,199456-56-9,108739-25-9,120329-57-9,120329-58-0
fullerene-C₆₀

: 150493-27-9
ethyl 3′H-cyclopropa[1,9](C₆₀-I_h)[5,6]fullerene-3′-carboxylate

: 161432-01-5
1,2-dihydrofullerene functionalized with ethylester acetate group

: C₆₆H₁₀O₃

: C₆₈H₁₄O₄

Guidance literature:: With zinc; In neat (no solvent); for 0.333333h; Ambient temperature;
DOI:10.1039/cc9960002059

Reference yield:

: 865-47-4
potassium tert-butylate

: 100-39-0
benzyl bromide

: 161432-01-5
1,2-dihydrofullerene functionalized with ethylester acetate group

: 1,4-dihydrofullerene functionalized with ethylester acetate group (R) and benzyl group (R')

Guidance literature:: potassium tert-butylate; 1,2-dihydrofullerene functionalized with ethylester acetate group; In tetrahydrofuran; at 20 ℃; for 1h;

benzyl bromide; In tetrahydrofuran; at 20 ℃; Further stages.;
DOI:10.1039/b207433h