2,3-dimethylphenyl phenyl sulfone

Base Information

• Chemical Name: 2,3-dimethylphenyl phenyl sulfone
• CAS No.: 28523-22-0
• Molecular Formula: C₁₄H₁₄O₂S
• Molecular Weight: 246.33
• Mol file: 28523-22-0.mol

Synonyms:

Chemical Property of 2,3-dimethylphenyl phenyl sulfone

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2,3-dimethylphenyl phenyl sulfone

There total 3 articles about 2,3-dimethylphenyl phenyl sulfone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

→ 2,3-dimethylphenyl phenyl sulfone (28523-22-0)

Guidance literature:

Reference yield:

o-xylene (95-47-6) + benzenesulfonyl chloride (98-09-9) → 3,4-dimethyl-1-(phenylsulphonyl)benzene (10355-01-8) + 2,3-dimethylphenyl phenyl sulfone (28523-22-0)

Guidance literature:

With tin(II) trifluoromethanesulfonate; at 120 ℃; for 8h;

DOI:10.1016/S0040-4020(00)01005-X

Reference yield:

o-xylene (95-47-6) + benzenesulfonic acid (98-11-3) → 3,4-dimethyl-1-(phenylsulphonyl)benzene (10355-01-8) + 2,3-dimethylphenyl phenyl sulfone (28523-22-0)

Guidance literature:

With silica gel-supported aluminum chloride; at 80 ℃; for 1.5h; regioselective reaction; Neat (no solvent);

DOI:10.1080/17415991003777391

upstream raw materials:

o-xylene

benzenesulfonyl chloride

benzenesulfonic acid