Technology Process of C28H25NO6S
There total 6 articles about C28H25NO6S which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
palladium 10% on activated carbon; ammonium formate; acetic acid;
at 125 ℃;
for 15h;
DOI:10.1007/s00044-010-9369-3
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: sulfuric acid / 15 h / Inert atmosphere; Reflux
2.1: sodium hydride / N,N-dimethyl-formamide
2.2: 18 h / 80 °C
3.1: piperidine; benzoic acid / toluene / 5 h / Reflux
4.1: palladium 10% on activated carbon; ammonium formate; acetic acid / 15 h / 125 °C
With
piperidine; sulfuric acid; palladium 10% on activated carbon; ammonium formate; sodium hydride; acetic acid; benzoic acid;
In
N,N-dimethyl-formamide; toluene;
3.1: Knoevenagel condensation;
DOI:10.1007/s00044-010-9369-3
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: sodium hydride / N,N-dimethyl-formamide
1.2: 18 h / 80 °C
2.1: piperidine; benzoic acid / toluene / 5 h / Reflux
3.1: palladium 10% on activated carbon; ammonium formate; acetic acid / 15 h / 125 °C
With
piperidine; palladium 10% on activated carbon; ammonium formate; sodium hydride; acetic acid; benzoic acid;
In
N,N-dimethyl-formamide; toluene;
2.1: Knoevenagel condensation;
DOI:10.1007/s00044-010-9369-3
