Y2(μ2-(CH3)3SiNC(C6H5)N(CH2)3NC(C6H5)NSi(CH3)3)3*DME

Base Information

Chemical Name:Y2(μ2-(CH3)3SiNC(C6H5)N(CH2)3NC(C6H5)NSi(CH3)3)3*DME
CAS No.:1041636-75-2
Molecular Formula:C₄H₁₀O₂*C₆₉H₁₀₂N₁₂Si₆Y₂
Molecular Weight:1536.1
Hs Code.:

Synonyms:

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Chemical Property of Y2(μ2-(CH3)3SiNC(C6H5)N(CH2)3NC(C6H5)NSi(CH3)3)3*DME

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Technology Process of Y2(μ2-(CH3)3SiNC(C6H5)N(CH2)3NC(C6H5)NSi(CH3)3)3*DME

There total 3 articles about Y2(μ2-(CH3)3SiNC(C6H5)N(CH2)3NC(C6H5)NSi(CH3)3)3*DME which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

: 110-71-4
1,2-dimethoxyethane

: 2Li⁽¹⁺⁾*((CH₃)3SiNC(C₆H₅)N)2(CH₂)3^(2-)*0.5C₄H₈O=((CH₃)3SiN(Li)C(C₆H₅)N)2(CH₂)3*0.5C₄H₈O

: 10361-92-9,61894-01-7
yttrium(III) chloride

: 1041636-75-2
Y2(μ2-(CH3)3SiNC(C6H5)N(CH2)3NC(C6H5)NSi(CH3)3)3*DME

Guidance literature:: In tetrahydrofuran; (Ar); a THF soln. of Li-complex added to stirring soln. of YCl3 in THF; volatiles removed under reduced pressure; extracted with toluene and evaporated to dry; dissolved in DME; filtered; cooling to 0°C;
DOI:10.1016/j.poly.2008.03.006

Reference yield: 62.0%

: 1041636-71-8
((CH₃)3SiNC(C₆H₅)N(CH₂)3NC(C₆H₅)NSi(CH₃)3)YCl(DME)

: 1041636-79-6
[Li(DME)3][Y((CH₃)3SiNC(C₆H₅)N(CH₂)3NC(C₆H₅)NSi(CH₃)3)2]

: 1041636-75-2
Y2(μ2-(CH3)3SiNC(C6H5)N(CH2)3NC(C6H5)NSi(CH3)3)3*DME

Guidance literature:: In tetrahydrofuran; (Ar); a clear soln. of Li-complex in THF added to a stirring soln. of YCl-complex in THF; volatiles removed under reduced pressure; extracted with toluene; evaporated to dry; dissolved in DME; filtered; cooling to 0°C;
DOI:10.1016/j.poly.2008.03.006

Reference yield: 55.0%

: 110-71-4
1,2-dimethoxyethane

: 2Li⁽¹⁺⁾*((CH₃)3SiNC(C₆H₅)N)2(CH₂)3^(2-)*0.5C₄H₈O=((CH₃)3SiN(Li)C(C₆H₅)N)2(CH₂)3*0.5C₄H₈O

: 1041636-71-8
((CH₃)3SiNC(C₆H₅)N(CH₂)3NC(C₆H₅)NSi(CH₃)3)YCl(DME)

: 1041636-75-2
Y2(μ2-(CH3)3SiNC(C6H5)N(CH2)3NC(C6H5)NSi(CH3)3)3*DME

Guidance literature:: In tetrahydrofuran; (Ar); a soln. of Li-complex in THF added to stirring soln. of Y-complex in THF; stirred for 48 h at room temp.; volatiles removed under reduced pressure; residue extracted with toluene; evaporated to dry; dissolved in DME; filtered; cooling to 0°C; elem. anal.;
DOI:10.1016/j.poly.2008.03.006