2-(3-bromophenoxy)benzonitrile

Base Information

• Chemical Name: 2-(3-bromophenoxy)benzonitrile
• CAS No.: 1020922-43-3
• Molecular Formula: C13H8 Br N O
• Molecular Weight: 274.117
• Mol file: 1020922-43-3.mol

Synonyms:

Chemical Property of 2-(3-bromophenoxy)benzonitrile

Chemical Property:

• PSA: 33.02000
• LogP: 4.11308

Purity/Quality:

99% ^*data from raw suppliers

2-(3-Bromophenoxy)benzonitrile 95% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2-(3-bromophenoxy)benzonitrile

There total 2 articles about 2-(3-bromophenoxy)benzonitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-bromo-6-fluorobenzonitrile (105942-08-3) + phenol (108-95-2,27073-41-2) → 5-bromo-phenoxybenzonitrile (1020922-43-3)

Guidance literature:

With potassium carbonate; In water; dimethyl sulfoxide;

Reference yield:

3-Bromophenol (591-20-8) + 2-fluorobenzonitrile (394-47-8) → 5-bromo-phenoxybenzonitrile (1020922-43-3)

Guidance literature:

With potassium carbonate; In N,N-dimethyl-formamide; at 100 ℃; for 10h; Inert atmosphere;

DOI:10.1002/anie.201706597

Reference yield: 67.0%

5-bromo-phenoxybenzonitrile (1020922-43-3) + bis(pinacol)diborane (73183-34-3) → 2-phenxoy-5-(4,4,5,5-tetramethyl-1,3,2-dioxaborolane-2-yl)benzonitrile + 2-phenoxy-5-(4,4,5,5-tetramethyl-1,3,2-dioxaborolane-2-yl)benzonitrile (364353-92-4)

Guidance literature:

With potassium acetate; In dichloromethane; N,N-dimethyl-formamide;

upstream raw materials:

4-bromo-6-fluorobenzonitrile

phenol

3-Bromophenol

2-fluorobenzonitrile

Downstream raw materials:

2-phenoxy-5-(4,4,5,5-tetramethyl-1,3,2-dioxaborolane-2-yl)benzonitrile

N-(3-bromophenyl)-2-hydroxy-N-methylbenzamide

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