2(e)-<3,4-Dibenzyloxy-phenyl>-3(a)-iod-trans-decalin-2a-isocyanat; (+/-)-<2c-(3,4-Dibenzyloxy-phenyl)-3c-iod-(4ar,8at)-decahydro-(2t)-naphthyl>-isocyanat

Base Information

Chemical Name:2(e)-<3,4-Dibenzyloxy-phenyl>-3(a)-iod-trans-decalin-2a-isocyanat; (+/-)-<2c-(3,4-Dibenzyloxy-phenyl)-3c-iod-(4ar,8at)-decahydro-(2t)-naphthyl>-isocyanat
CAS No.:32568-24-4
Molecular Formula:C₃₁H₃₂INO₃
Molecular Weight:593.504
Hs Code.:

2(e)-<3,4-Dibenzyloxy-phenyl>-3(a)-iod-trans-decalin-2a-isocyanat; (+/-)-<2c-(3,4-Dibenzyloxy-phenyl)-3c-iod-(4ar,8at)-decahydro-(2t)-naphthyl>-isocyanat

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Chemical Property of 2(e)-<3,4-Dibenzyloxy-phenyl>-3(a)-iod-trans-decalin-2a-isocyanat; (+/-)-<2c-(3,4-Dibenzyloxy-phenyl)-3c-iod-(4ar,8at)-decahydro-(2t)-naphthyl>-isocyanat

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Technology Process of 2(e)-<3,4-Dibenzyloxy-phenyl>-3(a)-iod-trans-decalin-2a-isocyanat; (+/-)-<2c-(3,4-Dibenzyloxy-phenyl)-3c-iod-(4ar,8at)-decahydro-(2t)-naphthyl>-isocyanat

There total 5 articles about 2(e)-<3,4-Dibenzyloxy-phenyl>-3(a)-iod-trans-decalin-2a-isocyanat; (+/-)-<2c-(3,4-Dibenzyloxy-phenyl)-3c-iod-(4ar,8at)-decahydro-(2t)-naphthyl>-isocyanat which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 16047-57-7
(((4-bromo-1,2-phenylene)bis(oxy))bis(methylene))dibenzene

: 32568-24-4
2(e)-<3,4-Dibenzyloxy-phenyl>-3(a)-iod-trans-decalin-2a-isocyanat; (+/-)-<2c-(3,4-Dibenzyloxy-phenyl)-3c-iod-(4ar,8at)-decahydro-(2t)-naphthyl>-isocyanat

Guidance literature:: Multi-step reaction with 2 steps

1: (i) Mg, THF, (ii) /BRN= 3195756/, Et₂O, (iii) KHSO₄, benzene

2: I₂ / diethyl ether; tetrahydrofuran

With iodine; In tetrahydrofuran; diethyl ether;
DOI:10.1021/jm00287a001

Reference yield:

: 10403-73-3
1,2-di(benzyloxy)benzene

: 32568-24-4
2(e)-<3,4-Dibenzyloxy-phenyl>-3(a)-iod-trans-decalin-2a-isocyanat; (+/-)-<2c-(3,4-Dibenzyloxy-phenyl)-3c-iod-(4ar,8at)-decahydro-(2t)-naphthyl>-isocyanat

Guidance literature:: Multi-step reaction with 3 steps

1: NBS / CCl₄

2: (i) Mg, THF, (ii) /BRN= 3195756/, Et₂O, (iii) KHSO₄, benzene

3: I₂ / diethyl ether; tetrahydrofuran

With N-Bromosuccinimide; iodine; In tetrahydrofuran; tetrachloromethane; diethyl ether;
DOI:10.1021/jm00287a001

Reference yield:

: 100-44-7
benzyl chloride

: 32568-24-4
2(e)-<3,4-Dibenzyloxy-phenyl>-3(a)-iod-trans-decalin-2a-isocyanat; (+/-)-<2c-(3,4-Dibenzyloxy-phenyl)-3c-iod-(4ar,8at)-decahydro-(2t)-naphthyl>-isocyanat

Guidance literature:: Multi-step reaction with 4 steps

1: K₂CO₃ / acetone

2: NBS / CCl₄

3: (i) Mg, THF, (ii) /BRN= 3195756/, Et₂O, (iii) KHSO₄, benzene

4: I₂ / diethyl ether; tetrahydrofuran

With N-Bromosuccinimide; iodine; potassium carbonate; In tetrahydrofuran; tetrachloromethane; diethyl ether; acetone;
DOI:10.1021/jm00287a001