N-Methyl-1-isochromancarboxanilid

Base Information

Chemical Name:N-Methyl-1-isochromancarboxanilid
CAS No.:83501-36-4
Molecular Formula:C₁₇H₁₇NO₂
Molecular Weight:267.327
Hs Code.:

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Suppliers and Price of N-Methyl-1-isochromancarboxanilid

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-Methyl-1-isochromancarboxanilid

Chemical Property:

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Technology Process of N-Methyl-1-isochromancarboxanilid

There total 1 articles about N-Methyl-1-isochromancarboxanilid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 13328-85-3
3,4-dihydro-1H-2-benzopyran-1-carboxylic acid

: 100-61-8
N-methylaniline

: 83501-36-4
N-Methyl-1-isochromancarboxanilid

Guidance literature:: With pyridine; thionyl chloride; N,N-dimethyl-formamide; Yield given. Multistep reaction; 1) 1 h, room temp., 30 min, 60 degC; 2) ether, 1 h, room temp.;

Reference yield:

: 83501-36-4
N-Methyl-1-isochromancarboxanilid

: 83501-56-8
1-Benzyl-1-isochromancarbaldehyd

Guidance literature:: Multi-step reaction with 2 steps

1: 75 percent / diisobutyl aluminium hydride / tetrahydrofuran; hexane / -40 °C

2: 1) NaH / 1) THF, 45 min; 2) 12 h, room temp.

With sodium hydride; diisobutylaluminium hydride; In tetrahydrofuran; hexane;