N^α'-Benzyloxycarbonyl-L-cystathionin-α'-methylester; (L-2-Amino-7-benzyloxycarbonylamino-4-thiaoctan-1-saeure-8-saeuremethylester

Base Information

• Chemical Name: N^α'-Benzyloxycarbonyl-L-cystathionin-α'-methylester; (L-2-Amino-7-benzyloxycarbonylamino-4-thiaoctan-1-saeure-8-saeuremethylester
• CAS No.: 15159-68-9
• Molecular Formula: C₁₆H₂₂N₂O₆S
• Molecular Weight: 370.426
• Mol file: 15159-68-9.mol

Synonyms:

Chemical Property of N^α'-Benzyloxycarbonyl-L-cystathionin-α'-methylester; (L-2-Amino-7-benzyloxycarbonylamino-4-thiaoctan-1-saeure-8-saeuremethylester

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of N^α'-Benzyloxycarbonyl-L-cystathionin-α'-methylester; (L-2-Amino-7-benzyloxycarbonylamino-4-thiaoctan-1-saeure-8-saeuremethylester

There total 3 articles about N^α'-Benzyloxycarbonyl-L-cystathionin-α'-methylester; (L-2-Amino-7-benzyloxycarbonylamino-4-thiaoctan-1-saeure-8-saeuremethylester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

α-amino-γ-bromobutyric acid methyl ester hydrochloride (15159-66-7) → Nα'-Benzyloxycarbonyl-L-cystathionin-α'-methylester; (L-2-Amino-7-benzyloxycarbonylamino-4-thiaoctan-1-saeure-8-saeuremethylester (15159-68-9)

Guidance literature:

Multi-step reaction with 2 steps

1: aq. NaHCO₃

2: (i) Na, liq. NH₃, (ii) /BRN= 2659160/, NH₄Cl

With sodium hydrogencarbonate;

Reference yield:

benzyl chloroformate (501-53-1,94274-21-2) → Nα'-Benzyloxycarbonyl-L-cystathionin-α'-methylester; (L-2-Amino-7-benzyloxycarbonylamino-4-thiaoctan-1-saeure-8-saeuremethylester (15159-68-9)

Guidance literature:

Multi-step reaction with 2 steps

1: aq. NaHCO₃

2: (i) Na, liq. NH₃, (ii) /BRN= 2659160/, NH₄Cl

With sodium hydrogencarbonate;

Reference yield:

L-cystine (56-89-3) + (2S)-2-benzyloxycarbonylamino-4-bromo-butyric acid methyl ester (15159-67-8) → Nα'-Benzyloxycarbonyl-L-cystathionin-α'-methylester; (L-2-Amino-7-benzyloxycarbonylamino-4-thiaoctan-1-saeure-8-saeuremethylester (15159-68-9)

Guidance literature:

Multistep reaction; (i) Na, liq. NH₃, (ii) /BRN= 2659160/, NH₄Cl;

upstream raw materials:

L-cystine

(2S)-2-benzyloxycarbonylamino-4-bromo-butyric acid methyl ester

α-amino-γ-bromobutyric acid methyl ester hydrochloride

benzyl chloroformate

Downstream raw materials:

N^α'-Benzyloxycarbonyl-L-cystathionin

(S)-2-Benzyloxycarbonylamino-4-((R)-2-tert-butoxycarbonylamino-2-carboxy-ethylsulfanyl)-butyric acid methyl ester

N^α'-benzyloxycarbonyl-cystathionine α-tert-butyl ester α'-methyl ester

N^α'-benzyloxycarbonylcystathionine α-tert-butyl ester