2,5-dimethoxy-3,4-β-trinitrostyrene

Base Information

• Chemical Name: 2,5-dimethoxy-3,4-β-trinitrostyrene
• CAS No.: 74422-84-7
• Molecular Formula: C₁₀H₉N₃O₈
• Molecular Weight: 299.197
• Mol file: 74422-84-7.mol

Synonyms:

Chemical Property of 2,5-dimethoxy-3,4-β-trinitrostyrene

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2,5-dimethoxy-3,4-β-trinitrostyrene

There total 2 articles about 2,5-dimethoxy-3,4-β-trinitrostyrene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 51.0%

2,5-dimethoxy-3,β-dinitrostyrene (74422-83-6) → 2,5-dimethoxy-3,4-β-trinitrostyrene (74422-84-7)

Guidance literature:

With nitric acid; at 0 ℃; for 0.333333h;

Reference yield:

2,5-dimethoxy-3-nitrobenzaldehyde (74422-90-5) → 2,5-dimethoxy-3,4-β-trinitrostyrene (74422-84-7)

Guidance literature:

Multi-step reaction with 2 steps

1: 1) KOH 2)acetic anhydride, sodium acetate / 1) water, ethanol, 5 deg C, 38 h 2) reflux 15 min.

2: 51 percent / 99percent nitric acid / 0.33 h / 0 °C

With potassium hydroxide; nitric acid; sodium acetate; acetic anhydride;

Reference yield:

2,5-dimethoxy-3,4-β-trinitrostyrene (74422-84-7) → 2,5-dimethoxy-3,4-diaminostyrene (74422-85-8)

Guidance literature:

With iron; acetic acid; In ethanol; for 0.666667h; Heating;

upstream raw materials:

2,5-dimethoxy-3,β-dinitrostyrene

2,5-dimethoxy-3-nitrobenzaldehyde

Downstream raw materials:

2,5-dimethoxy-3,4-diaminostyrene