2,5-dimethoxy-3,β-dinitrostyrene

Base Information

• Chemical Name: 2,5-dimethoxy-3,β-dinitrostyrene
• CAS No.: 74422-83-6
• Molecular Formula: C₁₀H₁₀N₂O₆
• Molecular Weight: 254.199
• Mol file: 74422-83-6.mol

Synonyms:

Chemical Property of 2,5-dimethoxy-3,β-dinitrostyrene

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2,5-dimethoxy-3,β-dinitrostyrene

There total 1 articles about 2,5-dimethoxy-3,β-dinitrostyrene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

nitromethane (75-52-5) + 2,5-dimethoxy-3-nitrobenzaldehyde (74422-90-5) → 2,5-dimethoxy-3,β-dinitrostyrene (74422-83-6)

Guidance literature:

With potassium hydroxide; sodium acetate; acetic anhydride; Yield given. Multistep reaction; 1) water, ethanol, 5 deg C, 38 h 2) reflux 15 min.;

Reference yield: 51.0%

2,5-dimethoxy-3,β-dinitrostyrene (74422-83-6) → 2,5-dimethoxy-3,4-β-trinitrostyrene (74422-84-7)

Guidance literature:

With nitric acid; at 0 ℃; for 0.333333h;

Reference yield:

2,5-dimethoxy-3,β-dinitrostyrene (74422-83-6) → 2,5-dimethoxy-3,4-diaminostyrene (74422-85-8)

Guidance literature:

Multi-step reaction with 2 steps

1: 51 percent / 99percent nitric acid / 0.33 h / 0 °C

2: powdered iron, acetic acid / ethanol / 0.67 h / Heating

With nitric acid; iron; acetic acid; In ethanol;

upstream raw materials:

nitromethane

2,5-dimethoxy-3-nitrobenzaldehyde

Downstream raw materials:

2,5-dimethoxy-3,4-β-trinitrostyrene

2,5-dimethoxy-3,4-diaminostyrene