naringenin-7-O-4-phthalonitrile

Base Information

Chemical Name:naringenin-7-O-4-phthalonitrile
CAS No.:1202524-76-2
Molecular Formula:C₂₃H₁₄N₂O₅
Molecular Weight:398.375
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of naringenin-7-O-4-phthalonitrile

Chemical Property:

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Technology Process of naringenin-7-O-4-phthalonitrile

There total 1 articles about naringenin-7-O-4-phthalonitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 31643-49-9
4-Nitrophthalonitrile

: 480-41-1
5,7-Dihydroxy-2-(4-hydroxy-phenyl)-chroman-4-on

: 1202524-76-2
naringenin-7-O-4-phthalonitrile

Guidance literature:: 4-Nitrophthalonitrile; 5,7-Dihydroxy-2-(4-hydroxy-phenyl)-chroman-4-on; With potassium carbonate; In dimethyl sulfoxide; for 72h; Inert atmosphere;

With hydrogenchloride; water; In dimethyl sulfoxide; pH=3; regioselective reaction; Cooling with ice;
DOI:10.1016/j.jorganchem.2009.09.012

Reference yield: 48.0%

: 1202524-76-2
naringenin-7-O-4-phthalonitrile

: 91-15-6
phthalonitrile

: 1202524-78-4
2-naringenin-7-O-phthalocyaninatozinc(II)

Guidance literature:: With 2-(N,N-dimethylamino)ethanol; zinc(II) chloride; at 135 ℃; for 4h; Inert atmosphere;
DOI:10.1016/j.jorganchem.2009.09.012

Reference yield: 48.0%

: 1202524-76-2
naringenin-7-O-4-phthalonitrile

: 91-15-6
phthalonitrile

: 7646-85-7,24359-56-6
zinc(II) chloride

: 1202524-78-4
2-naringenin-7-O-phthalocyaninatozinc(II)

Guidance literature:: In further solvent(s); (Ar), substituted phthalonitrile, ZnCl2 and phthalonitrile )1:1.7:1.7) dissolved in N,N-dimethylaminoethanol, heated at 135°C for 4 h; cooled to room temp., pptd.(CH3OH/H2O 1:1), washed (CH3OH/H2O 1:1, H2O),dried (vac.), dissolved (THF), absorbed on silica gel, extd.(hot THF), evapd., chromy.(silica gel - THF/hexane 3:2), elem. anal.;
DOI:10.1016/j.jorganchem.2009.09.012