tetrachloro(methyldiphenylphosphineimino)(methyldiphenylphosphine oxide)molybdenum(V)

Base Information

• Chemical Name: tetrachloro(methyldiphenylphosphineimino)(methyldiphenylphosphine oxide)molybdenum(V)
• CAS No.: 63286-75-9
• Molecular Formula: C₂₆H₂₆Cl₄MoNOP₂
• Molecular Weight: 668.198

Synonyms:

Chemical Property of tetrachloro(methyldiphenylphosphineimino)(methyldiphenylphosphine oxide)molybdenum(V)

Chemical Property:

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Technology Process of tetrachloro(methyldiphenylphosphineimino)(methyldiphenylphosphine oxide)molybdenum(V)

There total 2 articles about tetrachloro(methyldiphenylphosphineimino)(methyldiphenylphosphine oxide)molybdenum(V) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 20.0%

nitrogen(II) oxide (10102-43-9) + molybdenum(V) chloride (10241-05-1) + diphenyl(methyl)phosphine (1486-28-8) → [MoCl2(methyldiphenylphosphine)2(methyldiphenylphosphine oxide)] (63280-61-5) + tetrachloro(methyldiphenylphosphineimino)(methyldiphenylphosphine oxide)molybdenum(V) (63286-75-9) + amidotrichlorobis(methyldiphenylphosphine oxide)molybdenum(IV) chloride (63286-76-0)

Guidance literature:

With water; In benzene; N2-atmosphere; passing NO2 through soln. of MoCl5 (room temp., stirring,8 min), removal of NO (vac.), filtration, washing (C6H6), drying (0.01 Torr), suspending in C6H6, addn. of PMePh2, stirring (room temp., 1 h); water as impurity in solvent; filtration, evapn. of filtrate (reduced pressure), extn. with hexane, fractional crystn. of residue (CH2Cl2/hexane), washing (acetone), drying (0.01 Torr, room temp., 6 h); elem. anal.;

DOI:10.1039/DT9770000429

Reference yield: 20.0%

nitrogen(II) oxide (10102-43-9) + molybdenum(V) chloride (10241-05-1) + diphenyl(methyl)phosphine (1486-28-8) → [MoCl2(methyldiphenylphosphine)2(methyldiphenylphosphine oxide)] (63280-61-5) + tetrachloro(methyldiphenylphosphineimino)(methyldiphenylphosphine oxide)molybdenum(V) (63286-75-9)

Guidance literature:

In benzene; N2-atmosphere; passing NO2 through soln. of MoCl5 in dry benzene (room temp., stirring, 8 min), removal of NO (vac.), filtration, washing (benzene), drying (0.01 Torr), suspending in benzene, addn. of PMePh2, stirring (room temp., 1 h); filtration, evapn. of filtrate (reduced pressure), extn. with hexane, crystn. of residue (CH2Cl2/hexane);

DOI:10.1039/DT9770000429

Reference yield:

tetrachloro(methyldiphenylphosphineimino)(methyldiphenylphosphine oxide)molybdenum(V) (63286-75-9) → P(CH3)(C6H5)2H(1+)*MoCl4(OP(CH3)(C6H5)2)(1-)=[P(CH3)(C6H5)2H][MoCl4(OP(CH3)(C6H5)2)]

Guidance literature:

With water; In dichloromethane; N2-atmosphere;

DOI:10.1039/DT9770000429

upstream raw materials:

nitrogen(II) oxide

molybdenum(V) chloride

diphenyl(methyl)phosphine

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