amidotrichlorobis(methyldiphenylphosphine oxide)molybdenum(IV) chloride

Base Information

Chemical Name:amidotrichlorobis(methyldiphenylphosphine oxide)molybdenum(IV) chloride
CAS No.:63286-76-0
Molecular Formula:C₂₆H₂₈Cl₃MoNO₂P₂*Cl
Molecular Weight:686.213
Hs Code.:

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Chemical Property of amidotrichlorobis(methyldiphenylphosphine oxide)molybdenum(IV) chloride

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Technology Process of amidotrichlorobis(methyldiphenylphosphine oxide)molybdenum(IV) chloride

There total 1 articles about amidotrichlorobis(methyldiphenylphosphine oxide)molybdenum(IV) chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 20.0%

: 10102-43-9
nitrogen(II) oxide

: 10241-05-1
molybdenum(V) chloride

: 1486-28-8
diphenyl(methyl)phosphine

: 63280-61-5
[MoCl₂(methyldiphenylphosphine)2(methyldiphenylphosphine oxide)]

: 63286-75-9
tetrachloro(methyldiphenylphosphineimino)(methyldiphenylphosphine oxide)molybdenum(V)

: 63286-76-0
amidotrichlorobis(methyldiphenylphosphine oxide)molybdenum(IV) chloride

Guidance literature:: With water; In benzene; N2-atmosphere; passing NO2 through soln. of MoCl5 (room temp., stirring,8 min), removal of NO (vac.), filtration, washing (C6H6), drying (0.01 Torr), suspending in C6H6, addn. of PMePh2, stirring (room temp., 1 h); water as impurity in solvent; filtration, evapn. of filtrate (reduced pressure), extn. with hexane, fractional crystn. of residue (CH2Cl2/hexane), washing (acetone), drying (0.01 Torr, room temp., 6 h); elem. anal.;
DOI:10.1039/DT9770000429