6-Cyano-2-pyridine carboxylic acid methyl ester

Base Information

• Chemical Name: 6-Cyano-2-pyridine carboxylic acid methyl ester
• CAS No.: 98436-83-0
• Molecular Formula: C₈H₆N₂O₂
• Molecular Weight: 162.148
• Hs Code.: 2933399090
• Mol file: 98436-83-0.mol

Synonyms:6-CYANO-2-PYRIDINE CARBOXYLIC ACID METHYL ESTER;Picolinic acid, 6-cyano-, methyl ester (6CI);Methyl 6-cyanopyridine-2-carboxylate;Methyl 6-cyanopicolinate;6-Cyano-2-Pyridine Carboxylic Acid Methyl Ester 6-CYANO-2-PYRIDINE CARBOXYLIC ACID METHYL ESTER

Chemical Property of 6-Cyano-2-pyridine carboxylic acid methyl ester

Chemical Property:

• Vapor Pressure: 0.000321mmHg at 25°C
• Melting Point: 111-113.5 °C
• Boiling Point: 320.3°C at 760 mmHg
• PKA: -2.02±0.10(Predicted)
• Flash Point: 147.5°C
• PSA: 62.98000
• Density: 1.25g/cm³
• LogP: 0.73988
• Storage Temp.: Inert atmosphere,Room Temperature

Purity/Quality:

97% ^*data from raw suppliers

6-Cyano-2-pyridineCarboxylicAcidMethylEster ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 6-Cyano-2-pyridine carboxylic acid methyl ester

There total 3 articles about 6-Cyano-2-pyridine carboxylic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 51.0%

methyl 6-Bromopicolinate (26218-75-7) + copper(I) cyanide (544-92-3) → methyl 6-cyanopicolinate (98436-83-0)

Guidance literature:

In N,N-dimethyl-formamide; at 150 ℃; for 0.0833333h; Microwave irradiation;

DOI:10.1039/c1dt11627d

Reference yield:

methyl 6-Bromopicolinate (26218-75-7) + copper(l) cyanide → methyl 6-cyanopicolinate (98436-83-0)

Guidance literature:

With pyridine; at 116 ℃; for 4h;

DOI:10.1002/cmdc.201900172

Reference yield:

→ methyl 6-cyanopicolinate (98436-83-0)

Guidance literature:

Methylpicolinat-1-oxid (bp=160-162grad/2.5Torr), 1) Dimethylsulfat (-> 1-Methoxy-2-methoxycarbonylpyridiniummethylsulfat), 2) KCN, A., W.;

upstream raw materials:

methyl 6-Bromopicolinate

copper(I) cyanide

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