Technology Process of 4-<4-Methoxy-phenyl>-tropon
There total 10 articles about 4-<4-Methoxy-phenyl>-tropon which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 90 percent / diethyl ether / 3 h / Ambient temperature
2: 73 percent / 2 h / 180 °C
3: NaOMe / anodic oxidation; supplied electricity: 3.3 F/mol, anode potential: 1.1 V vs. SCE
4: aq. 10percent H2SO4
With
sulfuric acid; sodium methylate;
In
diethyl ether;
DOI:10.1016/S0040-4020(01)87049-6
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 83 percent / Et4NOTs, NaOMe / -10 - 0 °C / carbon rod electrodes, 5 A, 2.5 F/mol
2: 90 percent / diethyl ether / 3 h / Ambient temperature
3: 73 percent / 2 h / 180 °C
4: NaOMe / anodic oxidation; supplied electricity: 3.3 F/mol, anode potential: 1.1 V vs. SCE
5: aq. 10percent H2SO4
With
sulfuric acid; sodium methylate; tetraethylammonium tosylate;
In
diethyl ether;
DOI:10.1016/S0040-4020(01)87049-6
- Guidance literature:
-
Multi-step reaction with 6 steps
1: 98 percent / 1 h / 150 °C
2: 83 percent / Et4NOTs, NaOMe / -10 - 0 °C / carbon rod electrodes, 5 A, 2.5 F/mol
3: 90 percent / diethyl ether / 3 h / Ambient temperature
4: 73 percent / 2 h / 180 °C
5: NaOMe / anodic oxidation; supplied electricity: 3.3 F/mol, anode potential: 1.1 V vs. SCE
6: aq. 10percent H2SO4
With
sulfuric acid; sodium methylate; tetraethylammonium tosylate;
In
diethyl ether;
DOI:10.1016/S0040-4020(01)87049-6
