dimesityl-(N-methylanthranilatimido)germanium

Base Information

Chemical Name:dimesityl-(N-methylanthranilatimido)germanium
CAS No.:146699-03-8
Molecular Formula:C₂₆H₂₉GeNO₂
Molecular Weight:460.112
Hs Code.:

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Chemical Property of dimesityl-(N-methylanthranilatimido)germanium

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Technology Process of dimesityl-(N-methylanthranilatimido)germanium

There total 1 articles about dimesityl-(N-methylanthranilatimido)germanium which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 17.0%

: 146699-05-0
((CH₃)3C₆H₂)2Ge(Cl)NHC₆H₄CO₂CH₃

: 146699-03-8
dimesityl-(N-methylanthranilatimido)germanium

Guidance literature:: With tert.-butyl lithium; In tetrahydrofuran; pentane; benzene; byproducts: LiCl; addn. of 4.84mmol BuLi in pentane to a soln. of 4.84mmol Ge-compound in 8ml THF at -78°C (exclusion of moisture), 3h between -78 to -20°C, replacing of solvents by C6H6;; centrifugation (LiCl); recrystn. from ether at -30°C; elem. anal.;;
DOI:10.1021/om00028a008

Reference yield: 99.0%

: 67-56-1
methanol

: 146699-03-8
dimesityl-(N-methylanthranilatimido)germanium

: 146699-10-7
((CH₃)3C₆H₂)2Ge(OCH₃)NH(C₆H₄CO₂CH₃)

Guidance literature:: In benzene; addn. of a soln. of CH3OH in C6H6 (0.32mmol) to 32mmol Ge-compound in C6H6, stirring for 1h at 50°C;; evapn.;;
DOI:10.1021/om00028a008

Reference yield: 95.0%

: 146699-03-8
dimesityl-(N-methylanthranilatimido)germanium

: 1137-96-8,26505-49-7,201024-81-9
N-(benzylidene)aniline N-oxide

: 146699-15-2
((CH₃)3C₆H₂)2GeN(C₆H₄CO₂CH₃)CH(C₆H₅)N(C₆H₅)O

Guidance literature:: In benzene; heating 0.3mmol Ge-compound and 0.3mmol nitrone in 3ml C6H6 for 3d at 100°C in a sealed tube;; evapn., extn. with pentane; elem. anal.;;
DOI:10.1021/om00028a008