{RhIrCl₂(CO)2((C₆H₅)2PCH₂P(C₆H₅)2)2}

Base Information

Chemical Name:{RhIrCl₂(CO)2((C₆H₅)2PCH₂P(C₆H₅)2)2}
CAS No.:864653-70-3
Molecular Formula:C₅₂H₄₄Cl₂IrO₂P₄Rh
Molecular Weight:1190.85
Hs Code.:

{RhIrCl<sub>2</sub>(CO)2((C<sub>6</sub>H<sub>5</sub>)2PCH<sub>2</sub>P(C<sub>6</sub>H<sub>5</sub>)2)2}

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Chemical Property of {RhIrCl₂(CO)2((C₆H₅)2PCH₂P(C₆H₅)2)2}

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Technology Process of {RhIrCl₂(CO)2((C₆H₅)2PCH₂P(C₆H₅)2)2}

There total 1 articles about {RhIrCl₂(CO)2((C₆H₅)2PCH₂P(C₆H₅)2)2} which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: di(rhodium)tetracarbonyl dichloride

: chlorocarbonylbis(bis(diphenylphosphino)methane)iridium

: 864653-70-3,121472-19-3
dichlorodicarbonylbis(bis(diphenylphosphino)methane)2iridiumrhodium

Guidance literature:: In dichloromethane; the Ir compd. and the Rh compd. were combined, dissolved in CH2Cl2, stirred for 18 h and refluxed for 1 h under N2; addn. of diethylether, filtn., washing with diethylether and drying in vac.; elem. anal.;

Reference yield: 80.0%

: 14104-20-2
silver tetrafluoroborate

: 864653-70-3,121472-19-3
dichlorodicarbonylbis(bis(diphenylphosphino)methane)2iridiumrhodium

: {μ-chlorodicarbonylbis(bis(diphenylphosphino)methane)rhodiumiridium} BF4

Guidance literature:: In tetrahydrofuran; addn. of AgBF4 in THF to a suspn. of the RhIr compd. in THF and stirring for 30 min; concn., addn. of diethylether, evapn., dissolving in CH2Cl2, addn. of diethylether, filtn. and drying in vac.; elem. anal.;

Reference yield: 69.0%

: 864653-70-3,121472-19-3
{RhIrCl₂(CO)2((C₆H₅)2PCH₂P(C₆H₅)2)2}

: 135708-03-1
{RhIrI₂(CO)(CO)((C₆H₅)2PCH₂P(C₆H₅)2)2}

Guidance literature:: With KI; In methanol; dichloromethane; reacted for 2 h; solvents removed in vacuo, redissolved in CH2Cl2, filtered under N2, concd., Et2O added, cooled to 0°C, elem. anal.;