Phosphoric acid (2R,3R,4R,5R)-4-(tert-butyl-dimethyl-silanyloxy)-2-[(4-methoxy-phenyl)-diphenyl-methoxymethyl]-5-{4-[2-(4-nitro-phenyl)-ethoxy]-2-oxo-2H-pyrimidin-1-yl}-tetrahydro-furan-3-yl ester 2-(4-nitro-phenyl)-ethyl ester; compound with triethyl-amine

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Chemical Name:Phosphoric acid (2R,3R,4R,5R)-4-(tert-butyl-dimethyl-silanyloxy)-2-[(4-methoxy-phenyl)-diphenyl-methoxymethyl]-5-{4-[2-(4-nitro-phenyl)-ethoxy]-2-oxo-2H-pyrimidin-1-yl}-tetrahydro-furan-3-yl ester 2-(4-nitro-phenyl)-ethyl ester; compound with triethyl-amine
CAS No.:87875-26-1
Molecular Formula:C₆H₁₅N*C₅₁H₅₇N₄O₁₄PSi
Molecular Weight:1110.28
Hs Code.:

Phosphoric acid (2R,3R,4R,5R)-4-(tert-butyl-dimethyl-silanyloxy)-2-[(4-methoxy-phenyl)-diphenyl-methoxymethyl]-5-{4-[2-(4-nitro-phenyl)-ethoxy]-2-oxo-2H-pyrimidin-1-yl}-tetrahydro-furan-3-yl ester 2-(4-nitro-phenyl)-ethyl ester; compound with triethyl-amine

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Chemical Property of Phosphoric acid (2R,3R,4R,5R)-4-(tert-butyl-dimethyl-silanyloxy)-2-[(4-methoxy-phenyl)-diphenyl-methoxymethyl]-5-{4-[2-(4-nitro-phenyl)-ethoxy]-2-oxo-2H-pyrimidin-1-yl}-tetrahydro-furan-3-yl ester 2-(4-nitro-phenyl)-ethyl ester; compound with triethyl-amine

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Technology Process of Phosphoric acid (2R,3R,4R,5R)-4-(tert-butyl-dimethyl-silanyloxy)-2-[(4-methoxy-phenyl)-diphenyl-methoxymethyl]-5-{4-[2-(4-nitro-phenyl)-ethoxy]-2-oxo-2H-pyrimidin-1-yl}-tetrahydro-furan-3-yl ester 2-(4-nitro-phenyl)-ethyl ester; compound with triethyl-amine

There total 8 articles about Phosphoric acid (2R,3R,4R,5R)-4-(tert-butyl-dimethyl-silanyloxy)-2-[(4-methoxy-phenyl)-diphenyl-methoxymethyl]-5-{4-[2-(4-nitro-phenyl)-ethoxy]-2-oxo-2H-pyrimidin-1-yl}-tetrahydro-furan-3-yl ester 2-(4-nitro-phenyl)-ethyl ester; compound with triethyl-amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 100-27-6
2-(4-nitrophenyl)ethanol

: 87875-26-1
Phosphoric acid (2R,3R,4R,5R)-4-(tert-butyl-dimethyl-silanyloxy)-2-[(4-methoxy-phenyl)-diphenyl-methoxymethyl]-5-{4-[2-(4-nitro-phenyl)-ethoxy]-2-oxo-2H-pyrimidin-1-yl}-tetrahydro-furan-3-yl ester 2-(4-nitro-phenyl)-ethyl ester; compound with triethyl-amine

Guidance literature:: Multi-step reaction with 7 steps

1: 90 percent / SOCl₂, pyridine / 2 h / Heating

2: NaI / butan-2-one

3: 70 percent

4: NH₃ / methanol

5: 38 percent / imidazole / pyridine

With pyridine; 1H-imidazole; thionyl chloride; ammonia; sodium iodide; In pyridine; methanol; butanone;
DOI:10.1016/S0040-4039(00)88175-7

Reference yield:

: 20264-95-3
2-(4-nitrophenyl)ethyl chloride

: 87875-26-1
Phosphoric acid (2R,3R,4R,5R)-4-(tert-butyl-dimethyl-silanyloxy)-2-[(4-methoxy-phenyl)-diphenyl-methoxymethyl]-5-{4-[2-(4-nitro-phenyl)-ethoxy]-2-oxo-2H-pyrimidin-1-yl}-tetrahydro-furan-3-yl ester 2-(4-nitro-phenyl)-ethyl ester; compound with triethyl-amine

Guidance literature:: Multi-step reaction with 6 steps

1: NaI / butan-2-one

2: 70 percent

3: NH₃ / methanol

4: 38 percent / imidazole / pyridine

With 1H-imidazole; ammonia; sodium iodide; In pyridine; methanol; butanone;
DOI:10.1016/S0040-4039(00)88175-7

Reference yield:

: 20264-96-4
2-(4-nitrophenyl)ethyl iodide

: 87875-26-1
Phosphoric acid (2R,3R,4R,5R)-4-(tert-butyl-dimethyl-silanyloxy)-2-[(4-methoxy-phenyl)-diphenyl-methoxymethyl]-5-{4-[2-(4-nitro-phenyl)-ethoxy]-2-oxo-2H-pyrimidin-1-yl}-tetrahydro-furan-3-yl ester 2-(4-nitro-phenyl)-ethyl ester; compound with triethyl-amine

Guidance literature:: Multi-step reaction with 5 steps

1: 70 percent

2: NH₃ / methanol

3: 38 percent / imidazole / pyridine

With 1H-imidazole; ammonia; In pyridine; methanol;
DOI:10.1016/S0040-4039(00)88175-7