CpCr[(2,6-Me₂C₆H₃NCMe)2CH](I)

Base Information

Chemical Name:CpCr[(2,6-Me₂C₆H₃NCMe)2CH](I)
CAS No.:1198298-17-7
Molecular Formula:C₂₆H₃₀CrIN₂
Molecular Weight:549.438
Hs Code.:

CpCr[(2,6-Me<sub>2</sub>C<sub>6</sub>H<sub>3</sub>NCMe)2CH](I)

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Chemical Property of CpCr[(2,6-Me₂C₆H₃NCMe)2CH](I)

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Technology Process of CpCr[(2,6-Me₂C₆H₃NCMe)2CH](I)

There total 7 articles about CpCr[(2,6-Me₂C₆H₃NCMe)2CH](I) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.9%

: 1065614-63-2
CpCr[(XylNCMe)₂CH]

: 7553-56-2,12190-71-5,8031-47-8
iodine

: 1198298-17-7
CpCr[(2,6-Me₂C₆H₃NCMe)2CH](I)

Guidance literature:: In diethyl ether; under N2; soln. of I2 in Et2O added to soln. of Cr complex in Et2O; stirred overnight; solvent removed in vac.; extd. with Et2O; filtered through Celite; filtrate cooled to -30°C; crystals isolated in four crops over severald; elem. anal.;
DOI:10.1021/om900788c