N-(butylcarbamoyl)-1-phenylmethanesulfonamide

Base Information

• Chemical Name: N-(butylcarbamoyl)-1-phenylmethanesulfonamide
• CAS No.: 13909-67-6
• Molecular Formula: C₁₂H₁₈N₂O₃S
• Molecular Weight: 270.353
• Mol file: 13909-67-6.mol

Synonyms:Urea,1-(benzylsulfonyl)-3-butyl- (6CI,7CI,8CI); NSC 34011

Chemical Property of N-(butylcarbamoyl)-1-phenylmethanesulfonamide

Chemical Property:

• Density: 1.206g/cm³

Purity/Quality:

98%,99%, ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of N-(butylcarbamoyl)-1-phenylmethanesulfonamide

There total 6 articles about N-(butylcarbamoyl)-1-phenylmethanesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N-butyl-N'-phenylmethanesulfonyl-thiourea (93139-02-7) → N-Butyl-N'-phenylmethansulfonyl-harnstoff (13909-67-6)

Guidance literature:

With sodium hydroxide; dihydrogen peroxide;

Reference yield:

butyl isothiocyanate (592-82-5) → N-Butyl-N'-phenylmethansulfonyl-harnstoff (13909-67-6)

Guidance literature:

Multi-step reaction with 2 steps

2: aqueous H₂O₂; aq. NaOH solution

With sodium hydroxide; dihydrogen peroxide;

Reference yield:

N,N'-di-n-butylurea (1792-17-2) + sodium salt of phenylmethanesulfamide (57864-65-0) → N-Butyl-N'-phenylmethansulfonyl-harnstoff (13909-67-6)

Guidance literature:

at 190 ℃;

DOI:10.1039/j39670000701

upstream raw materials:

N-butyl-N'-phenylmethanesulfonyl-thiourea

phenyl methanesulfonyl carbamic acid ethylester

N-butylamine

N,N'-di-n-butylurea