4--arsenobenzen

Base Information

• Chemical Name: 4--arsenobenzen
• CAS No.: 4421-46-9
• Molecular Formula: C₂₀H₂₄As₂Cl₄N₂
• Molecular Weight: 584.079
• Mol file: 4421-46-9.mol

Synonyms:

Chemical Property of 4--arsenobenzen

Chemical Property:

Purity/Quality:

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Useful:

Technology Process of 4--arsenobenzen

There total 2 articles about 4--arsenobenzen which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N,N-Bis-(2-chloroethyl)-p-arsanilic Acid (5185-71-7) → 4--arsenobenzen (4421-46-9)

Guidance literature:

With hydrogenchloride; potassium iodide; tin(ll) chloride; In methanol;

DOI:10.1021/jm00320a016

Reference yield:

4-arsenoso-N,N-bis-(2-chloro-ethyl)-aniline cyclooligomers (4164-07-2) → 4--arsenobenzen (4421-46-9)

Guidance literature:

Multi-step reaction with 2 steps

1: H₂O₂, aq. NaOH

2: SnCl₂, aq. HCl, KI / methanol

With hydrogenchloride; sodium hydroxide; dihydrogen peroxide; potassium iodide; tin(ll) chloride; In methanol;

DOI:10.1021/jm00320a016

upstream raw materials:

N,N-Bis-(2-chloroethyl)-p-arsanilic Acid

4-arsenoso-N,N-bis-(2-chloro-ethyl)-aniline cyclooligomers