IndTi(OC₆H₃-2,6-(i)Pr₂)Me₂

Base Information

Chemical Name:IndTi(OC₆H₃-2,6-(i)Pr₂)Me₂
CAS No.:1075165-98-8
Molecular Formula:C₂₃H₃₀OTi
Molecular Weight:370.371
Hs Code.:

IndTi(OC<sub>6</sub>H<sub>3</sub>-2,6-(i)Pr<sub>2</sub>)Me<sub>2</sub>

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Chemical Property of IndTi(OC₆H₃-2,6-(i)Pr₂)Me₂

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Technology Process of IndTi(OC₆H₃-2,6-(i)Pr₂)Me₂

There total 1 articles about IndTi(OC₆H₃-2,6-(i)Pr₂)Me₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 84365-55-9
(η(5)-indenyl)trichlorotitanium

: 2078-54-8
2,6-diisopropylphenol

: 676-58-4
methylmagnesium chloride

: 1075165-98-8
IndTi(OC₆H₃-2,6-(i)Pr₂)Me₂

Guidance literature:: In tetrahydrofuran; dichloromethane; under N2 atm. to soln. IndTiCl3 in CH2Cl2 at -78°C soln. MeMgCl in THF was added and stirred for 1 h at -78°C, soln. phenol in CH2Cl2 was added dropwise, warmed to room temp. and stirred for 1 h; solvent was removed in vacuo, benzene was added, soln. was filtered through Celite and evapd. to dryness; elem. anal.;
DOI:10.1021/om8004993