N--carbaminsaeure-ethylester

Base Information

• Chemical Name: N--carbaminsaeure-ethylester
• CAS No.: 68871-52-3
• Molecular Formula: C₁₃H₁₇NO₅
• Molecular Weight: 267.282

Synonyms:

Chemical Property of N--carbaminsaeure-ethylester

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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Technology Process of N--carbaminsaeure-ethylester

There total 2 articles about N--carbaminsaeure-ethylester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

hydroxycarbamic acid ethyl ester; potassium salt (54149-30-3) + ethyl 2-phenyl-2-bromoacetate (2882-19-1,2216-90-2) → N--carbaminsaeure-ethylester (68871-52-3)

Guidance literature:

With potassium hydroxide; In ethanol; Heating;

Reference yield:

ethyl N-hydroxylcarbamate (589-41-3) + ethyl 2-phenyl-2-bromoacetate (2882-19-1,2216-90-2) → N--carbaminsaeure-ethylester (68871-52-3)

Guidance literature:

DOI:10.1016/0040-4020(78)88341-0

Reference yield:

N--carbaminsaeure-ethylester (68871-52-3) → N-(2-Hydroxy-1-phenyl-ethoxy)-carbaminsaeure-ethylester (68871-57-8)

Guidance literature:

With lithium aluminium tetrahydride;

DOI:10.1016/0040-4020(78)88341-0

upstream raw materials:

ethyl N-hydroxylcarbamate

ethyl 2-phenyl-2-bromoacetate

hydroxycarbamic acid ethyl ester; potassium salt

Downstream raw materials:

N-(2-Hydroxy-1-phenyl-ethoxy)-carbaminsaeure-ethylester

N-<1-Phenyl-1-ethoxycarbonyl-methoxy>-N-methyl-carbaminsaeure-ethylester

2-(aminooxy)-2-phenylethanol

(2-hydroxy-1-phenyl-ethoxy)-methyl-carbamic acid ethyl ester

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