isopropyl cinnamate

Base Information

Chemical Name:isopropyl cinnamate
CAS No.:131693-38-4
Molecular Formula:C₂₀H₁₇F₅O₃
Molecular Weight:400.345
Hs Code.:

isopropyl <m-(pentafluorobenzyloxy)-E-3-methyl>cinnamate

Synonyms:

Suppliers and Price of isopropyl cinnamate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of isopropyl cinnamate

Chemical Property:

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Technology Process of isopropyl cinnamate

There total 6 articles about isopropyl cinnamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 131693-35-1
m-(pentafluorobenzyloxy)-E-3-methylcinnamoyl chloride

: 67-63-0,8013-70-5
isopropyl alcohol

: 131693-38-4
isopropyl cinnamate

Guidance literature:: for 0.25h; Ambient temperature;
DOI:10.1016/S0040-4020(01)87912-6

Reference yield:

: 121-71-1
3-Hydroxyacetophenone

: 131693-38-4
isopropyl cinnamate

Guidance literature:: Multi-step reaction with 5 steps

1: 92 percent / aq.NaOH, tetra-n-butylammonium sulfate / CH₂Cl₂ / 3 h / Ambient temperature; similar yield with K₂CO₃ in acetone (reflux, 2 h)

2: 27 percent / xylene / 34 h / Heating

3: hydrolysis

4: 98 percent / SOCl₂ / benzene / 20 h / 90 °C

5: 95 percent / 0.25 h / Ambient temperature

With sodium hydroxide; thionyl chloride; tetrabutylammonium sulfate; In dichloromethane; xylene; benzene;
DOI:10.1016/S0040-4020(01)87912-6

Reference yield:

: 131693-26-0
m-(pentafluorobenzyloxy)acetophenone

: 131693-38-4
isopropyl cinnamate

Guidance literature:: Multi-step reaction with 4 steps

1: 27 percent / xylene / 34 h / Heating

2: hydrolysis

3: 98 percent / SOCl₂ / benzene / 20 h / 90 °C

4: 95 percent / 0.25 h / Ambient temperature

With thionyl chloride; In xylene; benzene;
DOI:10.1016/S0040-4020(01)87912-6