C₂₁H₃₂O₄

Base Information

Chemical Name:C₂₁H₃₂O₄
CAS No.:1300655-89-3
Molecular Formula:C₂₁H₃₂O₄
Molecular Weight:348.483
Hs Code.:

C<sub>21</sub>H<sub>32</sub>O<sub>4</sub>

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₁H₃₂O₄

Chemical Property:

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Technology Process of C₂₁H₃₂O₄

There total 5 articles about C₂₁H₃₂O₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 201230-82-2
carbon monoxide

: 1300655-88-2
C₂₄H₃₆O₂Si

: 1300655-89-3
C₂₁H₃₂O₄

Guidance literature:: carbon monoxide; C₂₄H₃₆O₂Si; With acetylacetonatodicarbonylrhodium(l); In benzene; at 60 ℃; for 4.5h; under 51716.2 Torr; Autoclave;

With potassium fluoride; dihydrogen peroxide; In tetrahydrofuran; methanol; water; at 40 ℃; for 1h; optical yield given as %de; diastereoselective reaction; Inert atmosphere;
DOI:10.1021/ja201467z

Reference yield:

: 1300655-86-0
C₁₃H₁₈O₂

: 1300655-89-3
C₂₁H₃₂O₄

Guidance literature:: Multi-step reaction with 3 steps

1.1: n-butyllithium / hexane; tert-butyl methyl ether / 0.17 h / -78 °C / Inert atmosphere

1.2: 0.67 h / 0 - 20 °C / Inert atmosphere

2.1: sodium hydride / hexane / 2 h / Inert atmosphere; Reflux

3.1: acetylacetonatodicarbonylrhodium(l) / benzene / 4.5 h / 60 °C / 51716.2 Torr / Autoclave

3.2: 1 h / 40 °C / Inert atmosphere

With acetylacetonatodicarbonylrhodium(l); n-butyllithium; sodium hydride; In hexane; tert-butyl methyl ether; benzene;
DOI:10.1021/ja201467z

Reference yield:

: 928-92-7
(E)-hex-4-en-1-ol

: 1300655-89-3
C₂₁H₃₂O₄

Guidance literature:: Multi-step reaction with 5 steps

1.1: sodium hydride / tetrahydrofuran / 0.17 h / 0 °C / Inert atmosphere

1.2: 12 h / 0 - 70 °C / Inert atmosphere

2.1: Oxone; Shi's ketone; tetra(n-butyl)ammonium hydrogensulfate; edetate disodium; potassium carbonate; acetic acid; potassium hydroxide / Dimethoxymethane; acetonitrile / 3 h / -10 °C / Inert atmosphere; aq. buffer

3.1: n-butyllithium / hexane; tert-butyl methyl ether / 0.17 h / -78 °C / Inert atmosphere

3.2: 0.67 h / 0 - 20 °C / Inert atmosphere

4.1: sodium hydride / hexane / 2 h / Inert atmosphere; Reflux

5.1: acetylacetonatodicarbonylrhodium(l) / benzene / 4.5 h / 60 °C / 51716.2 Torr / Autoclave

5.2: 1 h / 40 °C / Inert atmosphere

With Oxone; acetylacetonatodicarbonylrhodium(l); n-butyllithium; Shi's ketone; tetra(n-butyl)ammonium hydrogensulfate; edetate disodium; sodium hydride; potassium carbonate; acetic acid; potassium hydroxide; In tetrahydrofuran; Dimethoxymethane; hexane; tert-butyl methyl ether; acetonitrile; benzene;
DOI:10.1021/ja201467z