C₂₅H₂₀ClN₃O₂

Base Information

Chemical Name:C₂₅H₂₀ClN₃O₂
CAS No.:1261277-01-3
Molecular Formula:C₂₅H₂₀ClN₃O₂
Molecular Weight:429.906
Hs Code.:

C<sub>25</sub>H<sub>20</sub>ClN<sub>3</sub>O<sub>2</sub>

Synonyms:

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Chemical Property of C₂₅H₂₀ClN₃O₂

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Technology Process of C₂₅H₂₀ClN₃O₂

There total 3 articles about C₂₅H₂₀ClN₃O₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 90259-31-7
2-bromo-6-methylbenzoic acid

: 1261277-01-3
C₂₅H₂₀ClN₃O₂

Guidance literature:: Multi-step reaction with 4 steps

1: oxalyl dichloride / N,N-dimethyl-formamide / dichloromethane / 2 h / 20 °C

2: N-Bromosuccinimide; dibenzoyl peroxide / tetrachloromethane / 4 h / Reflux

3: N-ethyl-N,N-diisopropylamine / isopropyl alcohol / 20 - 150 °C / Microwave irradiation

4: sodium carbonate / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / ethanol; water / 0.25 h / 150 °C / Microwave irradiation

With N-Bromosuccinimide; oxalyl dichloride; sodium carbonate; N-ethyl-N,N-diisopropylamine; dibenzoyl peroxide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; N,N-dimethyl-formamide; In tetrachloromethane; ethanol; dichloromethane; water; isopropyl alcohol; 4: Suzuki Coupling;

Reference yield:

: 99548-56-8
methyl 2-bromo-6-methyl-benzoate

: 1261277-01-3
C₂₅H₂₀ClN₃O₂

Guidance literature:: Multi-step reaction with 3 steps

1: N-Bromosuccinimide; dibenzoyl peroxide / tetrachloromethane / 4 h / Reflux

2: N-ethyl-N,N-diisopropylamine / isopropyl alcohol / 20 - 150 °C / Microwave irradiation

3: sodium carbonate / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / ethanol; water / 0.25 h / 150 °C / Microwave irradiation

With N-Bromosuccinimide; sodium carbonate; N-ethyl-N,N-diisopropylamine; dibenzoyl peroxide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrachloromethane; ethanol; water; isopropyl alcohol; 3: Suzuki Coupling;

Reference yield:

: 777859-74-2
methyl?2-bromo-6-(bromomethyl)benzoate

: 1261277-01-3
C₂₅H₂₀ClN₃O₂

Guidance literature:: Multi-step reaction with 2 steps

1: N-ethyl-N,N-diisopropylamine / isopropyl alcohol / 20 - 150 °C / Microwave irradiation

2: sodium carbonate / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / ethanol; water / 0.25 h / 150 °C / Microwave irradiation

With sodium carbonate; N-ethyl-N,N-diisopropylamine; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In ethanol; water; isopropyl alcohol; 2: Suzuki Coupling;