C₇H₃BrClIO

Base Information

Chemical Name:C₇H₃BrClIO
CAS No.:1261470-90-9
Molecular Formula:C₇H₃BrClIO
Molecular Weight:345.362
Hs Code.:

Synonyms:

Suppliers and Price of C₇H₃BrClIO

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₇H₃BrClIO

Chemical Property:

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Technology Process of C₇H₃BrClIO

There total 3 articles about C₇H₃BrClIO which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 7149-03-3
ethyl 3-bromo-4-aminobenzoate

: 1261470-90-9
C₇H₃BrClIO

Guidance literature:: Multi-step reaction with 3 steps

1.1: sulfuric acid; sodium nitrite / water / 2 h / 0 °C / Inert atmosphere

1.2: 0 - 20 °C / Inert atmosphere

2.1: water; sodium hydroxide / tetrahydrofuran / 2 h / 20 °C / Inert atmosphere

3.1: thionyl chloride / toluene / 14 h / 20 °C / Inert atmosphere; Reflux

With thionyl chloride; sulfuric acid; water; sodium hydroxide; sodium nitrite; In tetrahydrofuran; water; toluene;
DOI:10.1002/anie.201106734

Reference yield:

: 94-09-7
p-aminoethylbenzoate

: 1261470-90-9
C₇H₃BrClIO

Guidance literature:: Multi-step reaction with 4 steps

1.1: N-Bromosuccinimide / chloroform / 3 h / 0 °C / Inert atmosphere

2.1: sulfuric acid; sodium nitrite / water / 2 h / 0 °C / Inert atmosphere

2.2: 0 - 20 °C / Inert atmosphere

3.1: water; sodium hydroxide / tetrahydrofuran / 2 h / 20 °C / Inert atmosphere

4.1: thionyl chloride / toluene / 14 h / 20 °C / Inert atmosphere; Reflux

With N-Bromosuccinimide; thionyl chloride; sulfuric acid; water; sodium hydroxide; sodium nitrite; In tetrahydrofuran; chloroform; water; toluene;
DOI:10.1002/anie.201106734

Reference yield:

: 386267-31-8
ethyl 3-bromo-4-iodobenzoate

: 1261470-90-9
C₇H₃BrClIO

Guidance literature:: Multi-step reaction with 2 steps

1: water; sodium hydroxide / tetrahydrofuran / 2 h / 20 °C / Inert atmosphere

2: thionyl chloride / toluene / 14 h / 20 °C / Inert atmosphere; Reflux

With thionyl chloride; water; sodium hydroxide; In tetrahydrofuran; toluene;
DOI:10.1002/anie.201106734