4-hydroxy-5-phenylthio-N-benzylpentanamide

Base Information

Chemical Name:4-hydroxy-5-phenylthio-N-benzylpentanamide
CAS No.:117768-66-8
Molecular Formula:C₁₈H₂₁NO₂S
Molecular Weight:315.436
Hs Code.:

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Chemical Property of 4-hydroxy-5-phenylthio-N-benzylpentanamide

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Technology Process of 4-hydroxy-5-phenylthio-N-benzylpentanamide

There total 5 articles about 4-hydroxy-5-phenylthio-N-benzylpentanamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 108078-64-4
5-[(phenylsulfanyl)methyl]dihydrofuran-2(3H)-2-one

: 100-46-9
benzylamine

: 117768-66-8
4-hydroxy-5-phenylthio-N-benzylpentanamide

Guidance literature:: In tetrahydrofuran; for 72h; Heating;

Reference yield:

: 882-33-7
diphenyldisulfane

: 117768-66-8
4-hydroxy-5-phenylthio-N-benzylpentanamide

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) manganese(III) acetate dihydrate, trifluoroacetic acid, 2.) 15 percent aq. sodium carbonate / 1.) CH₂Cl₂, 0 deg C, 8 h, 2.) ether, rt, 18 h

2: 90 percent / cobalt(II) chloride hexahydrate / H₂O / 5 h / 170 °C

3: 77 percent / tetrahydrofuran / 72 h / Heating

With manganese triacetate; sodium carbonate; trifluoroacetic acid; cobalt(II) chloride; In tetrahydrofuran; water;

Reference yield:

: 592-51-8
4-Pentenenitrile

: 117768-66-8
4-hydroxy-5-phenylthio-N-benzylpentanamide

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) manganese(III) acetate dihydrate, trifluoroacetic acid, 2.) 15 percent aq. sodium carbonate / 1.) CH₂Cl₂, 0 deg C, 8 h, 2.) ether, rt, 18 h

2: 86 percent / cobalt(II) chloride hexahydrate / H₂O / 5 h / 170 °C

3: 77 percent / tetrahydrofuran / 72 h / Heating

With manganese triacetate; sodium carbonate; trifluoroacetic acid; cobalt(II) chloride; In tetrahydrofuran; water;