5-chloro-2-hydroxyacetophenone phenylhydrazone

Base Information

Chemical Name:5-chloro-2-hydroxyacetophenone phenylhydrazone
CAS No.:67338-35-6
Molecular Formula:C14H13ClN2O
Molecular Weight:260.72
Hs Code.:
Mol file:67338-35-6.mol

Synonyms:5-chloro-2-hydroxyacetophenone phenylhydrazone;5 - Chloro - 2 - hydroxyacetophenone phenylhydrazone;2'-Hydroxy-5'-chloracetophenon-phenylhydrazon;

Suppliers and Price of 5-chloro-2-hydroxyacetophenone phenylhydrazone

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 5 raw suppliers

Chemical Property of 5-chloro-2-hydroxyacetophenone phenylhydrazone

Chemical Property:

PSA：44.62000
LogP:3.95470

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 5-chloro-2-hydroxyacetophenone phenylhydrazone

There total 4 articles about 5-chloro-2-hydroxyacetophenone phenylhydrazone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1450-74-4
5-chloro-2-hydroxyacetophenone

: 100-63-0
phenylhydrazine

: 67338-35-6
4-chloro-2-[1-(2-phenylhydrazin-1-ylidene)ethyl]phenol

Guidance literature:: In acetic acid; Heating;

Reference yield:

: 876-27-7
4-chlorophenyl acetate

: 67338-35-6
4-chloro-2-[1-(2-phenylhydrazin-1-ylidene)ethyl]phenol

Guidance literature:: Multi-step reaction with 2 steps

1: aluminum (III) chloride / 30 h / 120 - 160 °C

2: acetic acid / ethanol / 4 h / Reflux

With aluminum (III) chloride; acetic acid; In ethanol; 1: |Fries Phenol Ester Rearrangement;

Reference yield:

: 106-48-9,82344-39-6
4-chloro-phenol

: 67338-35-6
4-chloro-2-[1-(2-phenylhydrazin-1-ylidene)ethyl]phenol

Guidance literature:: Multi-step reaction with 3 steps

1: sodium hydroxide

2: aluminum (III) chloride / 30 h / 120 - 160 °C

3: acetic acid / ethanol / 4 h / Reflux

With aluminum (III) chloride; acetic acid; sodium hydroxide; In ethanol; 2: |Fries Phenol Ester Rearrangement;