Technology Process of
silyl>(trimethylsilyl)diazomethan
There total 8 articles about silyl>(trimethylsilyl)diazomethan which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
at 50 ℃;
for 22h;
- Guidance literature:
-
With
chloro-trimethyl-silane;
In
benzene;
at 70 ℃;
for 2h;
Yield given. Yields of byproduct given. Title compound not separated from byproducts;
- Guidance literature:
-
Multi-step reaction with 2 steps
1: BuLi / diethyl ether; hexane / -78 °C
2: 34 percent Spectr. / 22 h / 50 °C
With
n-butyllithium;
In
diethyl ether; hexane;
