7-Bromo-3-chloro-5H-benzo[4,5]cyclohepta[1,2-B]pyridin-5-one

Base Information

Chemical Name:7-Bromo-3-chloro-5H-benzo[4,5]cyclohepta[1,2-B]pyridin-5-one
CAS No.:917878-65-0
Molecular Formula:C14H7BrClNO
Molecular Weight:320.573
Hs Code.:2933990090
DSSTox Substance ID:DTXSID30580582
Mol file:917878-65-0.mol

Synonyms:917878-65-0;7-BROMO-3-CHLORO-5H-BENZO[4,5]CYCLOHEPTA[1,2-B]PYRIDIN-5-ONE;7-Bromo-3-chloro-5H-benzo[4,5]cyclohepta-[1,2-b]pyridin-5-one;14-bromo-5-chloro-7-azatricyclo[9.4.0.03,8]pentadeca-1(11),3(8),4,6,9,12,14-heptaen-2-one;7-bromo-3-chloro-5H-benzo(4,5)cyclohenta(1,2-b)pyridin-5-one;SCHEMBL399570;DTXSID30580582;BREDBBFHVAQHCD-UHFFFAOYSA-N;AKOS015834678;CS-0119790;A15910;F52305;3-chloro-7-bromo-5H-benzo[4,5]cyclohepta[1,2-b]pyridin-5-one;14-bromo-5-chloro-7-azatricyclo[9.4.0.0^{3,8]pentadeca-1(11),3(8),4,6,9,12,14-heptaen-2-one

Suppliers and Price of 7-Bromo-3-chloro-5H-benzo[4,5]cyclohepta[1,2-B]pyridin-5-one

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Matrix Scientific
7-Bromo-3-chloro-5H-benzo[4,5]cyclohepta-[1,2-b]pyridin-5-one 95+%
250mg
$ 591.00

Matrix Scientific
7-Bromo-3-chloro-5H-benzo[4,5]cyclohepta-[1,2-b]pyridin-5-one 95+%
1g
$ 1311.00

Crysdot
7-Bromo-3-chloro-5H-benzo[4,5]cyclohepta[1,2-b]pyridin-5-one 95+%
1g
$ 594.00

Chemenu
7-Bromo-3-chloro-5H-benzo[4,5]cyclohepta-[1,2-b]pyridin-5-one 95%
1g
$ 1178.00

American Custom Chemicals Corporation
7-BROMO-3-CHLORO-5H-BENZO[4,5]CYCLOHEPTA[1,2-B]PYRIDIN-5-ONE 95.00%
5MG
$ 496.45

Alichem
7-Bromo-3-chloro-5H-benzo[4,5]cyclohepta[1,2-b]pyridin-5-one
1g
$ 1285.20

AK Scientific
7-Bromo-3-chloro-5H-benzo[4,5]cyclohepta[1,2-b]pyridin-5-one
250mg
$ 847.00

Total 19 raw suppliers

Chemical Property of 7-Bromo-3-chloro-5H-benzo[4,5]cyclohepta[1,2-B]pyridin-5-one

Chemical Property:

Vapor Pressure:1.22E-08mmHg at 25°C
Boiling Point:459.9°C at 760 mmHg
Flash Point:231.9°C
PSA：29.96000
Density:1.644g/cm³
LogP:4.16410
Storage Temp.:2-8°C
XLogP3:4.1
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:0
Exact Mass:318.93995
Heavy Atom Count:18
Complexity:373

Purity/Quality:

97% ^*data from raw suppliers

7-Bromo-3-chloro-5H-benzo[4,5]cyclohepta-[1,2-b]pyridin-5-one 95+% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC(=CC2=C1C=CC3=C(C2=O)C=C(C=N3)Cl)Br

Technology Process of 7-Bromo-3-chloro-5H-benzo[4,5]cyclohepta[1,2-B]pyridin-5-one

There total 6 articles about 7-Bromo-3-chloro-5H-benzo[4,5]cyclohepta[1,2-B]pyridin-5-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: 1170702-73-4
2-[(E)-2-(4-bromophenyl)vinyl]-5-chloronicotinic acid

: 917878-65-0
7-bromo-3-chloro-5H-benzo[4,5]cyclohepta[1,2-b]pyridin-5-one

Guidance literature:: 2-[(E)-2-(4-bromophenyl)vinyl]-5-chloronicotinic acid; at 180 - 220 ℃; Inert atmosphere; Large scale reaction;

With triethylamine; In dichloromethane; for 1h; Large scale reaction;
DOI:10.1021/op100101q

Reference yield: 35.0%

: 917942-73-5
C₁₄H₉BrClNO₂

: 917878-65-0
7-bromo-3-chloro-5H-benzo[4,5]cyclohepta[1,2-b]pyridin-5-one

Guidance literature:: With polyphosphoric acid; at 200 ℃; Inert atmosphere;
DOI:10.1021/jm200112k

Reference yield:

: 917882-51-0
2-[(E/Z)-2-(4-bromophenyl)vinyl]-3-carboxy-5-chloropyridinium chloride

: 917878-65-0
7-bromo-3-chloro-5H-benzo[4,5]cyclohepta[1,2-b]pyridin-5-one

Guidance literature:: 2-[(E/Z)-2-(4-bromophenyl)vinyl]-3-carboxy-5-chloropyridinium chloride; With PPA; at 200 ℃; for 12h;

With sodium hydroxide; In water;