METHYL6-METHOXY-2-PYRAZINECARBOXYLATE

Base Information

• Chemical Name: METHYL6-METHOXY-2-PYRAZINECARBOXYLATE
• CAS No.: 23813-24-3
• Molecular Formula: C7H8N2O3
• Molecular Weight: 168.15002
• Hs Code.: 2933990090
• Mol file: 23813-24-3.mol

Synonyms:6-Methoxypyrazine-2-carboxylic acid methyl ester;2-Methoxy-6-pyrazinecarboxylic acid methyl ester;

Chemical Property of METHYL6-METHOXY-2-PYRAZINECARBOXYLATE

Chemical Property:

• Vapor Pressure: 0.022mmHg at 25°C
• Melting Point: 81.5-82℃
• Boiling Point: 249.9±35.0℃ (760 Torr)
• PKA: -1.36±0.10(Predicted)
• Flash Point: 105.0±25.9℃
• PSA: 61.31000
• Density: 1.220±0.06 g/cm3 (20 ºC 760 Torr)
• LogP: 0.27180
• Storage Temp.: 2-8°C

Purity/Quality:

99%, ^*data from raw suppliers

Methyl6-Methoxy-2-pyrazinecarboxylate ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of METHYL6-METHOXY-2-PYRAZINECARBOXYLATE

There total 3 articles about METHYL6-METHOXY-2-PYRAZINECARBOXYLATE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

6-oxo-1,6-dihydro-pyrazine-2-carboxylic acid (13924-99-7) → 6-methoxypyrazine-2-carboxylic acid methyl ester (23813-24-3)

Guidance literature:

With chloro-trimethyl-silane; In methanol;

Reference yield:

sodium methylate (124-41-4) + 6-chloropyrazine-2-carbonitrile (6863-74-7) → 6-methoxypyrazine-2-carboxylic acid methyl ester (23813-24-3)

Guidance literature:

sodium methylate; 6-chloropyrazine-2-carbonitrile; In methanol; for 0.25h;

With hydrogenchloride; In methanol; at 20 ℃; for 0.5h; Further stages.;

DOI:10.3987/COM-06-10867

Reference yield:

→ 6-methoxypyrazine-2-carboxylic acid methyl ester (23813-24-3)

Guidance literature:

NaOMe, Carboxylat XII;

upstream raw materials:

sodium methylate

6-chloropyrazine-2-carbonitrile

6-oxo-1,6-dihydro-pyrazine-2-carboxylic acid

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