4-chloro-6-(α-hydroxyiminobenzyl)-1,3-O,O-ditosylresorcinol

Base Information

Chemical Name:4-chloro-6-(α-hydroxyiminobenzyl)-1,3-O,O-ditosylresorcinol
CAS No.:146963-12-4
Molecular Formula:C₂₇H₂₂ClNO₇S₂
Molecular Weight:572.059
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-chloro-6-(α-hydroxyiminobenzyl)-1,3-O,O-ditosylresorcinol

Chemical Property:

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Technology Process of 4-chloro-6-(α-hydroxyiminobenzyl)-1,3-O,O-ditosylresorcinol

There total 4 articles about 4-chloro-6-(α-hydroxyiminobenzyl)-1,3-O,O-ditosylresorcinol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 7051-13-0
1-chloro-2,4-dimethoxybenzene

: 146963-12-4
4-chloro-6-(α-hydroxyiminobenzyl)-1,3-O,O-ditosylresorcinol

Guidance literature:: Multi-step reaction with 3 steps

1: AlCl₃ / 1,2-dichloro-ethane / 0 deg C to RT, 3 h, then 50 deg C, 1 h

2: pyridine / 2 h / Heating

3: NH₂OH*HCl, pyridine / 3 h / Heating

With pyridine; aluminium trichloride; hydroxylamine hydrochloride; In 1,2-dichloro-ethane;
DOI:10.1248/cpb.40.2597

Reference yield:

: 151-10-0
1,3-Dimethoxybenzene

: 146963-12-4
4-chloro-6-(α-hydroxyiminobenzyl)-1,3-O,O-ditosylresorcinol

Guidance literature:: Multi-step reaction with 4 steps

1: SO₂Cl₂ / CHCl₃ / Ambient temperature

2: AlCl₃ / 1,2-dichloro-ethane / 0 deg C to RT, 3 h, then 50 deg C, 1 h

3: pyridine / 2 h / Heating

4: NH₂OH*HCl, pyridine / 3 h / Heating

With pyridine; aluminium trichloride; sulfuryl dichloride; hydroxylamine hydrochloride; In chloroform; 1,2-dichloro-ethane;
DOI:10.1248/cpb.40.2597