Technology Process of 4-chloro-6-(α-hydroxyiminobenzyl)-1,3-O,O-ditosylresorcinol
There total 4 articles about 4-chloro-6-(α-hydroxyiminobenzyl)-1,3-O,O-ditosylresorcinol which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 3 steps
1: AlCl3 / 1,2-dichloro-ethane / 0 deg C to RT, 3 h, then 50 deg C, 1 h
2: pyridine / 2 h / Heating
3: NH2OH*HCl, pyridine / 3 h / Heating
With
pyridine; aluminium trichloride; hydroxylamine hydrochloride;
In
1,2-dichloro-ethane;
DOI:10.1248/cpb.40.2597
- Guidance literature:
-
Multi-step reaction with 4 steps
1: SO2Cl2 / CHCl3 / Ambient temperature
2: AlCl3 / 1,2-dichloro-ethane / 0 deg C to RT, 3 h, then 50 deg C, 1 h
3: pyridine / 2 h / Heating
4: NH2OH*HCl, pyridine / 3 h / Heating
With
pyridine; aluminium trichloride; sulfuryl dichloride; hydroxylamine hydrochloride;
In
chloroform; 1,2-dichloro-ethane;
DOI:10.1248/cpb.40.2597
- Guidance literature:
-
With
pyridine; hydroxylamine hydrochloride;
for 3h;
Yield given;
Heating;
DOI:10.1248/cpb.40.2597
